首页> 外国专利> SOL-GEL FABRICATION METHOD OF CATALYST FOR SYNTHESIZING THIN MULTIWALLED CARBONNANOTUBE AND CARBONNANOTUBE MASS SYNTHESIZING METHOD USING THE CATALYST

SOL-GEL FABRICATION METHOD OF CATALYST FOR SYNTHESIZING THIN MULTIWALLED CARBONNANOTUBE AND CARBONNANOTUBE MASS SYNTHESIZING METHOD USING THE CATALYST

机译:薄壁多级碳纳米管催化剂的溶胶凝胶制备方法及使用该方法的碳纳米管质量合成方法

摘要

A method for producing catalytic for synthesizing a fraction wall multi-walls carbon nanotube is provided to synthesize massively a fraction wall multi-walls carbon nanotube of which purity is high, a diameter is 3 - 10 nm and a number of graphite wall is less. A method for producing catalytic for synthesizing a fraction wall multi-walls carbon nanotube comprises steps of: (S1) dissolving raw materials of iron and magnesium and a chelate agent in water; (S2) adding a raw material of molybdenum in a solution in which the raw material of the iron and the raw material of magnesium are dissolved; (S3) mixing the raw material of the iron and the raw material of the magnesium and the chelate agent and the raw material of the molybdenum while being heated at predetermined temperature; (S4) heating in order to diversified the raw material of the iron and the raw material of the magnesium and the chelate agent and the raw material of the molybdenum are mixed to a gel state material; (S5) heating up the gel state material and being diversified to the solid material; (S6) being diversified to powder by grinding a solid material; and (S7) reducing the powder under a hydrogen atmosphere.
机译:提供了一种用于合成级分壁多壁碳纳米管的催化剂的生产方法,以大规模合成纯度高,直径为3-10nm且石墨壁数较少的级分壁多壁碳纳米管。一种用于合成馏分壁多壁碳纳米管的催化剂的生产方法,包括以下步骤:(S1)将铁和镁的原料和螯合剂溶解在水中; (S2)在使铁的原料和镁的原料溶解的溶液中添加钼的原料。 (S3)在预定温度下加热的同时将铁的原料和镁的原料以及螯合剂和钼的原料混合; (S4)为了使铁的原料和镁的原料多样化而进行加热,将螯合剂和钼的原料混合成凝胶状的原料。 (S5)加热凝胶态材料,使其多样化为固体材料; (S6)通过研磨固体材料而分散成粉末; (S7)在氢气氛下还原粉末。

著录项

  • 公开/公告号KR20080105969A

    专利类型

  • 公开/公告日2008-12-04

    原文格式PDF

  • 申请/专利权人 JEIO CO LTD.;

    申请/专利号KR20080003606

  • 发明设计人 LEE CHEOL JIN;KANG DEUK JOO;

    申请日2008-01-11

  • 分类号B01J37/08;B01J23/745;B01J23/02;B82B3;

  • 国家 KR

  • 入库时间 2022-08-21 19:14:33

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