首页> 外国专利> MANUFACTURING METHOD FOR POLYIMIDE-BASED CARBON NANOFIBER ELECTRODE AND CARBON NANOTUBE COMPOSITE ELECTRODE AND CDI APPARATUS USING THE SAME

MANUFACTURING METHOD FOR POLYIMIDE-BASED CARBON NANOFIBER ELECTRODE AND CARBON NANOTUBE COMPOSITE ELECTRODE AND CDI APPARATUS USING THE SAME

机译:聚酰亚胺基碳纳米纤维电极和碳纳米管复合电极及CDI装置的制造方法

摘要

A method for manufacturing flat polyimide carbon nano fiber and carbon nanotube composite electrode are provided to minimize the diameter of the carbon fiber by using triethylamine as a catalyst and to improve the specific surface area of electrode. A method for manufacturing carbon fiber electrode comprises the steps of: (S20) synthesizing a polyamic acid which is the polyimide precursor by using pyromellitic dianhydride and oxydianiline as a monomer and triethylamine as catalyst; (S30) manufacturing spinning solution by putting dimethylformamide into the polyamic acid solution and obtaining polyamic acid nanofiber paper through electrostatic spinning; (S40) converting the polyamic acid nanofiber paper into polyimide through heat-treatment; and (S50) converting the polyimide nanofiber paper into carbon nanofiber through heat-treatment in the inert gas atmosphere.
机译:提供一种制造扁平聚酰亚胺碳纳米纤维和碳纳米管复合电极的方法,以通过使用三乙胺作为催化剂来使碳纤维的直径最小化并改善电极的比表面积。一种碳纤维电极的制造方法,包括以下步骤:(S20)以均苯四甲酸二酐和羟二苯胺为单体,以三乙胺为催化剂,合成作为聚酰亚胺前体的聚酰胺酸。 (S30)将二甲基甲酰胺放入聚酰胺酸溶液中,通过静电纺丝得到聚酰胺酸纳米纤维纸,制造纺丝液; (S40)通过热处理将聚酰胺酸纳米纤维纸转化为聚酰亚胺; (S50)通过在惰性气体气氛中进行热处理将聚酰亚胺纳米纤维纸转变为碳纳米纤维。

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