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Method for making carbon fibers, modified multiwall carbon nanotubes

机译:碳纤维的制造方法,改性多壁碳纳米管

摘要

FIELD: production processes.;SUBSTANCE: method involves drawing of carbon fibre through solution with further heat treatment in flow-through gas medium. As solution there used is either solution containing pre-synthesised thin multi-layered carbon nanotubes functionalised with hydroxylic and carboxylic groups in dimethyl formamide or in dimethyl acetamide or in dimethyl sulfoxide with concentration of 0.1-10 g/l, or catalytic solution containing medium for forming embryos for growing nanotubes at heat treatment, and as catalytic solution there used is water solution Co(NO3)2 with concentration of 0.25 mol/l. As gas medium there used is medium containing gaseous hydrocarbon - methane, and heat treatment is performed by keeping it in reactor at temperature of 800-1000°C during 10-30 minutes.;EFFECT: increasing resistance to fibres being drawn from binding material.;4 cl, 5 ex, 6 dwg
机译:领域:生产工艺;实质:该方法涉及通过在流通气体介质中进行进一步热处理的溶液拉伸碳纤维。作为溶液,可以使用含有预先合成的,由二甲基甲酰胺或二甲基乙酰胺或二甲亚砜中的羟基和羧基官能化的多层多层薄碳纳米管组成的溶液,其浓度为0.1-10 g / l,或者含有催化介质的催化溶液。在热处理时形成用于生长纳米管的胚,并且使用浓度为0.25 mol / l的水溶液Co(NO 3 2 作为催化溶液。作为气体介质,使用的是含有气态烃-甲烷的介质,并通过将其在反应器中于800-1000°C的温度下保持10-30分钟来进行热处理。效果:增加对从粘合材料中拉出纤维的抵抗力。 ; 4 cl,5 ex,6 dwg

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