首页> 外国专利> METHOD OF MONOAZO DYE E102 EXTRACTION FROM WATER SOLUTIONS IN PRESENCE OF MONOAZO DYE E122

METHOD OF MONOAZO DYE E102 EXTRACTION FROM WATER SOLUTIONS IN PRESENCE OF MONOAZO DYE E122

机译:存在莫诺唑染料E122时从水溶液中提取莫诺唑染料E102的方法

摘要

FIELD: chemistry.;SUBSTANCE: invention refers to the analytical chemistry of organic compounds with respect to monoazo dye extraction from water media. The method includes: a) the addition of the crystalline ammonium sulphate to the water solution of monoazo dye E102 and E122 mixture up to its concentration 43 wt %; b) separation by filtering of the monoazo dye E122 segregated due to desalting; c) acetone addition to the filtrate in volume ratio acetone: water solution = 1:10 and d) monoazo dye E102 extraction during 10 min and separation of the water phase. The content of monoazo dye E102 in water phase is determined spectrophotometrically; the rate of extraction (R%) was calculated by formula: R= [(Ainit-Aequil)*100%]/Ainit, where Ainit, Aequil are filtrate optical densities before and after filtration.;EFFECT: invention provides the maximal completeness of the extraction.;1 ex
机译:技术领域本发明涉及有机化合物相对于从水介质中提取单偶氮染料的分析化学。该方法包括:a)将结晶硫酸铵添加到单偶氮染料E102和E122混合物的水溶液中,直至其浓度为43重量%; b)通过过滤分离由于脱盐而分离的单偶氮染料E122; c)以丙酮:水溶液= 1∶10的体积比将丙酮加入滤液中,d)在10分钟内萃取单偶氮染料E102并分离水相。分光光度法测定水相中单偶氮染料E102的含量。萃取率(R%)的计算公式为:R = [(A init -A equil )* 100%] / A init ,其中A init ,A equil 是过滤前后的滤液光密度。效果:本发明提供了提取的最大完整性。

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