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MOISTURE MEASURING COULOMETRIC TITRATOR

机译:水分测定库仑滴定仪

摘要

PROBLEM TO BE SOLVED: To provide a moisture measuring coulometric titrator which can automatically inject a batchwise sample in succession and continuously perform a larger number of measurements in the moisture measuring coulometric titrator for measuring the moisture content of a liquid sample by a Karl Fischer method.;SOLUTION: The moisture measuring coulometric titrator includes a reagent circulating line for circulating a reagent into a titration cell (1), a metering pipe (6) for sampling a definite amount of a sample, a sample supply line for passing the sample through the metering pipe (6), and a flow channel switching valve (5). The flow channel switching valve (5) is constituted so as to switch a sample injecting flow channel wherein the metering pipe (6) is incorporated in the sample supply line and a moisture measuring flow channel wherein the metering pipe (6) is incorporated in the reagent circulating line and a gas supply line [flow channel (46)] for supplying a moisture non-containing pushing-out gas when batchwise measurement is completed is connected to the reagent circulating line [flow channel (41)] and constituted so as to recover the reagent in the metering pipe (6) in the titration cell (1) by the pushing-out gas.;COPYRIGHT: (C)2010,JPO&INPIT
机译:要解决的问题:提供一种水分测量库仑滴定仪,该滴定仪可以连续自动地分批注入样品,并在水分测量库仑滴定仪中连续进行大量测量,以通过卡尔·费休方法测量液体样品的水分含量。 ;解决方案:湿度测量库仑滴定仪包括用于将试剂循环到滴定池(1)中的试剂循环管线,用于对一定量的样品进行采样的计量管(6),用于使样品通过样品池的样品供应管线。计量管(6)和流道切换阀(5)。所述流路切换阀(5)构成为切换在所述样品供给管路内装有计量管(6)的试样注入流路和在所述供液管路内装有计量管(6)的水分测定流路。试剂循环管路[流路(41)]连接有试剂循环管路和气体供应管路[流路(46)],用于在分批测量完成时供应不含水分的推出气体。通过顶出气体回收滴定池(1)中计量管(6)中的试剂。版权所有:(C)2010,JPO&INPIT

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