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METHOD FOR DETECTING PARAFFIN WAX AND ASPHALTENE CONTENT IN OIL

机译:石油中石蜡和沥青质含量的检测方法

摘要

This invention relates to geology, geochemistry, oil refinery and petroleum chemistry and can be implemented for determination of paraffin and asphaltene concentration in oil, in particular, for analysis of heavy oils and bitumens. To determine concentration of paraffins and asphaltenes in oil, three crude oil samples are extracted; two extracted samples are dissolved in a solvent and the solvent alongside with light oil fractions is then removed; meanwhile, asphaltenes are removed from one of the solvent-treated samples. A nucleic magnetic resonance method is employed for measuring free inductance drop-down curves for all three samples; thereafter, a ratio of solid hydrogen-containing fractions suspended in oil, to liquid hydrogen-containing fractions is defined. The paraffin concentration is judged by the content of solid hydrogen-containing fractions in the solvent-treated sample, from which asphaltenes have been removed. The asphaltene concentration is judged by the content of solid hydrogen-containing fractions in the other solvent-treated sample, with the consideration of the defined concentration of paraffins. The concentration of paraffins and asphaltenes in original oil is determined based on the defined paraffin-to-asphaltene ratio in solid hydrogen-containing fractions.
机译:本发明涉及地质,地球化学,炼油厂和石油化学,并且可用于测定油中石蜡和沥青质的浓度,特别是用于重油和沥青的分析。为了确定油中链烷烃和沥青质的浓度,提取了三个原油样品;最后,提取了三个样品。将两次提取的样品溶解在溶剂中,然后除去溶剂和轻油馏分;同时,从其中一种溶剂处理过的样品中去除了沥青质。核磁共振法用于测量所有三个样品的自由电感下降曲线。此后,确定悬浮在油中的固体含氢馏分与液体含氢馏分的比例。通过溶剂处理过的样品中已除去沥青质的固体含氢馏分的含量来判断石蜡浓度。沥青质浓度是由另一种溶剂处理过的样品中固体含氢馏分的含量来判断的,同时要考虑到所定义的石蜡浓度。根据定义的固体含氢馏分中石蜡与沥青质的比例,确定原始油中石蜡和沥青质的浓度。

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