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METHOD FOR MAKING BIODEGRADABLE CERAMIC COMPOSITE OF DOUBLE POTASSIUM CALCIUM PHOSPHATE

机译:磷酸二钾钙的生物可降解陶瓷复合材料的制备方法

摘要

FIELD: medicine.;SUBSTANCE: there is described a method for making a biodegradable ceramic composite of double potassium calcium phosphate that involves preparation of a initial powder containing calcium phosphate with the ratio Ca/P=1 and potassium sa extrusion and burning, wherein according to the invention, the initial powder is formed by the reaction at pH 5.5-6.0 of aqueous solutions of calcium acetate and potassium hydrophosphate concentrated within 0.6-0.8 M. The powder after the synthesis represents mixed calcium-deficient hydroxyapatite, brushite and acid potassium acetate.;EFFECT: use of said mixture after burning allows making the biodegradable ceramic composite exhibiting the uniform microstructure with the size of grains 2-4 mcm, of double potassium calcium phosphate Ca10K(PO4)7, containing TCP phase.;3 cl, 1 tbl, 2 dwg, 1 ex
机译:领域:描述了一种制备双磷酸钙磷酸钙的可生物降解的陶瓷复合材料的方法,该方法包括制备包含Ca / P = 1的磷酸钙和钾盐的初始粉末。挤压和燃烧,其中根据本发明,初始粉末是通过在pH 5.5-6.0的条件下,将乙酸钙和磷酸氢钾水溶液浓缩在0.6-0.8 M范围内反应而形成的。合成后的粉末表示混合的缺钙羟基磷灰石效果:燃烧后使用上述混合物可使生物可降解陶瓷复合材料显示出均匀的微观结构,晶粒尺寸为2-4 mcm,是双磷酸钙钙Ca 10 K(PO 4 7 ,包含TCP相位; 3 cl,1 tbl,2 dwg,1 ex

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