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METHOD FOR PRODUCING 2-ANILINO-4,6-DIMETHYLPYRIMIDINE

机译:生产2-苯胺基-4,6-二甲基嘧啶的方法

摘要

The invention relates to a method for producing 2-anilino-4,6-dimethylpyrimidine by reacting phenylguanidine and/or one of its salts with acetylacetone in the presence of water and/or without removing amounts of water that are produced by the reaction. For the reaction that is preferably carried out at pressures ranging between 0.1 and 10 bar and at temperatures between 40 and 180 °C, especially phenylguanidine carbonate and phenylguanidine hydrogen carbonate are used, preferably moistened with water. The invention provides a method for obtaining, by means of a technically simple method and under environmentally friendly conditions, in very good yields a fine-grained product that has excellent purity.
机译:本发明涉及一种通过在水的存在下和/或不除去反应产生的水的条件下使苯基胍和/或其盐之一与乙酰丙酮反应来制备2-苯胺基-4,6-二甲基嘧啶的方法。对于优选在0.1至10巴的压力和40至180℃的温度下进行的反应,尤其使用碳酸苯胍和碳酸苯胍碳酸氢盐,优选用水润湿。本发明提供了一种方法,该方法通过技术上简单的方法并且在环境友好的条件下以非常好的收率获得了具有优异纯度的细粒产品。

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