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MANUFACTURING METHOD OF DODECACALCIUM HEPTA-ALUMINATE AND DODECACALCIUM HEPTA-ALUMINATE MANUFACTURED BY THE METHOD

机译:庚二酸十二钙的制造方法及该方法制造的庚二酸十二盐的制造方法

摘要

PURPOSE: A method for manufacturing dodecacalcium hepta-aluminate and the dodecacalcium hepta-aluminate prepared using the same are provided to simplify a manufacturing process and obtain the high reproducibility. CONSTITUTION: An aluminum-tri-sec-butoxide is mixed with ethylacetoacetate or acetyl acetone to prepare a chelated aluminum alkoxide solution. A first organic solvent is added to melt the chelated aluminum alkoxide solution. Distilled water is added to the first organic solvent mixed with the chelated aluminum alkoxide solution in order to implement a hydrolysis reaction. An acid solution, which does not form salt with respect to the chelated aluminum alkoxide solution, is added to prepare an alumina source solution.
机译:目的:提供一种十二烷基铝酸十二钙的制造方法,以及使用该方法制备的十二烷基铝酸十二盐,以简化制造过程并获得高再现性。组成:将三仲丁醇铝与乙酰乙酸乙酯或乙酰丙酮混合以制备螯合的烷氧基铝溶液。添加第一有机溶剂以使螯合的烷氧基铝溶液熔融。将蒸馏水加入与螯合的烷氧基铝溶液混合的第一有机溶剂中以进行水解反应。加入相对于螯合的醇铝溶液不形成盐的酸溶液,以制备氧化铝源溶液。

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