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Low-temperature method of producing nano-scaled graphene platelets and their nanocomposites

机译:低温制备纳米石墨烯薄片及其纳米复合材料的方法

摘要

A method of exfoliating a layered material to produce separated nano-scaled platelets having a thickness smaller than 100 nm. The method comprises: (a) providing a graphite intercalation compound comprising a layered graphite containing expandable species residing in an interlayer space of the layered graphite; (b) exposing the graphite intercalation compound to an exfoliation temperature lower than 650° C. for a duration of time sufficient to at least partially exfoliate the layered graphite without incurring a significant level of oxidation; and (c) subjecting the at least partially exfoliated graphite to a mechanical shearing treatment to produce separated platelets. The method can further include a step of dispersing the platelets in a polymer or monomer solution or suspension as a precursor step to nanocomposite fabrication.
机译:一种剥离层状材料以产生厚度小于100 nm的分离的纳米级血小板的方法。该方法包括:(a)提供一种石墨插层化合物,其包括层状石墨,该层状石墨包含位于层状石墨的层间空间中的可膨胀物质。 (b)将石墨插层化合物暴露于低于650℃的剥离温度的持续时间足以至少部分剥离层状石墨而不会引起显着的氧化水平; (c)对至少部分剥离的石墨进行机械剪切处理以产生分离的血小板。该方法可以进一步包括将血小板分散在聚合物或单体溶液或悬浮液中的步骤,作为纳米复合材料制造的前体步骤。

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