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Method of preparing a transmission electron microscope sample and a sample piece for a transmission electron microscope

机译:制备透射电子显微镜样品的方法和用于透射电子显微镜的样品片

摘要

Provided is a method of preparing a sample piece for a transmission electron microscope, the sample piece for a transmission electron microscope including a substantially planar finished surface which can be observed with the transmission electron microscope and a grabbing portion which microtweezers can grab without contacting the finished surface. The method of preparing a sample piece for a transmission electron microscope is characterized by including: a first step of cutting out the sample piece from a sample body Wa with a charged particle beam, the sample piece being coupled to the sample body at a coupling portion; a second step of grabbing with the microtweezers the grabbing portion of the sample piece with the finished surface of the sample piece cut out in the first step being covered with the microtweezers; a third step of detaching the sample piece grabbed with the microtweezers in the second step from the sample body by cutting the coupling portion with the charged particle beam with a grabbed state of the sample piece being maintained; and a fourth step of transferring and fixing with the microtweezers the sample piece detached in the third step onto a sample holder.
机译:提供一种制备用于透射电子显微镜的样品片的方法,该用于透射电子显微镜的样品片包括可以用透射电子显微镜观察的基本平坦的精加工表面以及微镊子可以在不接触精加工剂的情况下进行抓取的抓取部分。表面。制备用于透射电子显微镜的样品片的方法的特征在于包括:第一步骤:用带电粒子束从样品体Wa中切出样品片,该样品片在结合部处与样品体结合。 ;第二步,用微镊子抓紧样品件的抓握部分,在第一步中切出的样品的精加工表面被微镊子覆盖;第三步骤是,在保持有样品片的抓握状态的状态下,通过切断带电粒子束的结合部,将第二步骤中被微镊子抓住的样品片从样品主体上取下。第四步骤是用微镊子将在第三步骤中分离的样品转移并固定到样品架上。

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