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Method for producing hydrophilic siloxanyl monomers cationic

机译:阳离子型亲水性硅氧烷基单体的制备方法

摘要

A forming monomer removable medical device obtainable cationic water by SomeProcedure comprising the steps of: providing a compound containing siloxane hydride, dissolving the compound containing siloxane hydride in a solvent or combination of solvents; treating compound siloxane contains hydride dissolved with an allyl halide and a catalyst conventionally dehidrolización to form a first reaction mixture; heating the first reaction mixture in a nitrogen atmosphere for a time sufficient to darcomo result a quantitative loss of reactants as determined by a technique analíticaapropiada thereby providing a monomer mixture; cooling the monomer mixture, concentrating the cooled mixture, dissolving in a suitable solvent cooled to nucleophilic substitution mixture, treating the cooled mixture containing the solvent suitable for nucleophilic substitution with u n compuestode amino-vinyl tertiary, to form a second reaction mixture; heating the second reaction mixture at a temperature sufficient to promote reaction without provocargelificación; remove any remaining solvent to provide a product containing material ypurificar material containing product to produce a device-forming monomer médicosextraíbles water.
机译:可通过SomeProcedure获得阳离子水的可除去单体的成型医疗器械,其包括以下步骤:提供含硅氧烷氢化物的化合物,将含硅氧烷氢化物的化合物溶解在溶剂或溶剂的组合中;处理化合物硅氧烷包含溶解有烯丙基卤化物的氢化物和按常规方法脱氢的催化剂以形成第一反应混合物;将第一反应混合物在氮气气氛中加热足以使达科莫反应的时间,从而导致反应物的定量损失,这是通过一种分析方法确定的,从而提供了单体混合物;冷却单体混合物,浓缩冷却的混合物,溶解在冷却成亲核取代混合物的合适的溶剂中,用Compuestode氨基-乙烯基叔叔胺处理包含适于亲核取代的溶剂的冷却混合物,以形成第二反应混合物;将第二反应混合物加热至足以促进反应而没有引发凝胶的温度;除去任何残留的溶剂,以提供一种含有产物的物质。含有多种物质的产物可以产生一种可形成装置的单体,该混合物可产生水。

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