首页> 外国专利> A method of producing toluene diisocyanate (TDI) in the process of the toluene diamine (TDA) phosgenation reaction in the gaseous phase

A method of producing toluene diisocyanate (TDI) in the process of the toluene diamine (TDA) phosgenation reaction in the gaseous phase

机译:在气相中甲苯二胺(TDA)光气化反应过程中生产甲苯二异氰酸酯(TDI)的方法

摘要

The invention relates to the method for producing toluene diisocyanate (TDI) in the process of toluene diamine phosgenation (TDA) in the gaseous phase, which uses toluene diamine (TDA) contaminated with solids as a substrate.;According to the invention, a method for producing toluene diisocyanate TDI in the phosgenation process of toluene diamine TDA, in the gaseous phase, characterised by the fact that as one of the substrates, non-distilled toluene diamine TDA is used, which contains up to 4% by weight of non-volatile substances, and the process of toluene diamine (TDA) evaporation is carried out in a thin film evaporator that is equipped with scrapers placed on the rotor, wherein the non-volatile substances in the toluene diamine TDA derived from toluene diamine TDA decomposition in conditions of carrying raw material conversion to the gas phase are carried away into the space located at the bottom of the evaporator 1.
机译:本发明涉及气相中甲苯二胺光气化(TDA)过程中甲苯二异氰酸酯(TDI)的生产方法,该方法以被固体污染的甲苯二胺(TDA)为底物。用于在气相二甲苯二胺TDA的光气化过程中生产甲苯二异氰酸酯TDI,其特征在于以下事实:使用一种非蒸馏的甲苯二胺TDA作为底物之一,其中含有高达4%重量的非二甲苯挥发性物质,甲苯二胺(TDA)的蒸发过程是在装有刮刀的薄膜蒸发器上进行的,该刮板放置在转子上,其中甲苯二胺TDA中的非挥发性物质在一定条件下由甲苯二胺TDA分解而来携带原料转化成气相的过程被带走到位于蒸发器1底部的空间中。

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