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METHOD FOR SYNTHESIZING SSZ-74 ZEOLITE AND SSZ-74 ZEOLITE SYNTHESIZED THEREFROM

机译:SSZ-74沸石的合成方法和SSZ-74沸石的合成方法

摘要

PURPOSE: A method for manufacturing SSZ-74 zeolite and the SSZ-74 zeolite manufactured by the same are provided to apply micro-porosity and meso-porosity to the SSZ-74 zeolite by adjusting the amount of bases during a hydrothermal synthesizing process. CONSTITUTION: Hydrous gel containing silica, the oxide of a trivalent atom, 1,1'-(pentane-1,5-diyl)bis(1-methylpyrrolidine-1-ium) as a structure directing agent, basic materials, and water is prepared(S10). The hydrous gel is hydrothermal reacted to form a solid product(S12). The solid product is calcined at 400-700 degrees Celsius to eliminate the structure directing agent(S20). The oxide of the trivalent atom is selected from a group including aluminum oxide, boric oxide, gallium oxide, indium oxide, zirconium oxide, vanadium oxide, titanium oxide, iron oxide, molybdenum oxide, manganese oxide, and a mixture of the same.
机译:目的:提供一种SSZ-74沸石的制造方法和由其制造的SSZ-74沸石,以通过在水热合成过程中调节碱的量来对SSZ-74沸石施加微孔和中孔。组成:含水凝胶,包含二氧化硅,三价原子的氧化物,1,1'-(戊烷-1,5-二基)双(1-甲基吡咯烷-1-鎓)作为结构导向剂,基础材料和水为准备(S10)。使含水凝胶水热反应以形成固体产物(S12)。将固体产物在400-700摄氏度下煅烧以消除结构定向剂(​​S20)。三价原子的氧化物选自氧化铝,氧化硼,氧化镓,氧化铟,氧化锆,氧化钒,氧化钛,氧化铁,氧化钼,氧化锰以及它们的混合物。

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