首页> 外国专利> MANUFACTURING METHOD OF HIGH POROUS LITHIUM MANGANESE OXIDE BASED EPOXY SPHERICAL COMPOSITE USING A TEMPLATE CARBONIZATION AND A SPRAY-DRYING METHOD CAPABLE OF IMPROVING ELECTRICAL ADSORPTION AND DESORPTION

MANUFACTURING METHOD OF HIGH POROUS LITHIUM MANGANESE OXIDE BASED EPOXY SPHERICAL COMPOSITE USING A TEMPLATE CARBONIZATION AND A SPRAY-DRYING METHOD CAPABLE OF IMPROVING ELECTRICAL ADSORPTION AND DESORPTION

机译:基于模板碳的高孔隙度氧化锰酸锂基环氧树脂球形复合材料的制备方法及能改善电吸附和脱附的喷雾干燥方法

摘要

PURPOSE: A manufacturing method of high porous lithium manganese oxide based epoxy spherical composite using a template carbonization and a spray-drying method are provided to synthesize lithium manganese oxide having low-density, large specific surface area, and high porosity.;CONSTITUTION: A manufacturing method of lithium manganese oxide based epoxy spherical composite comprises the following steps: mixing a binder resin composition with an inorganic compound; spraying the mixture on a fluorinated plate and manufacturing a spherical shaped composite by heat-treating; and acid processing the spherical shaped composite. The lithium manganese oxide based spherical shaped composite has a specific surface area of 40-60m^2/g and a pore volume range of 0.20-0. 40cm^3/g. The heating is processed at 450-520 deg. Celsius for 3-6 hours. In the mixing step, the binder resin composition comprises 5-15 parts by weight of imidazole based compound and 80-100 parts by weight of epoxy resin based on 100.0, parts by weight of phenol type curing agent. 30-70 wt% of solvent is included based on 100.0 wt% of the total weight portion. In the mixing step, the binder resin composition and the inorganic compound are mixed at a weight ratio of 1:1-3:1.;COPYRIGHT KIPO 2012
机译:目的:提供一种利用模板碳化的高多孔锂锰氧化物基环氧球形复合材料的制造方法和喷雾干燥法,以合成低密度,大比表面积和高孔隙率的锂锰氧化物。锂锰氧化物基环氧球形复合材料的制造方法包括以下步骤:将粘合剂树脂组合物与无机化合物混合;将混合物喷涂在氟化板上,并通过热处理制备球形复合材料。然后酸处理球形复合材料。锂锰氧化物基球形复合材料的比表面积为40-60m 2 / g,孔体积范围为0.20-0。 40厘米^ 3 /克。加热在450-520度下进行。摄氏3-6小时。在混合步骤中,基于100.0重量份的酚类固化剂,粘合剂树脂组合物包含5-15重量份的咪唑基化合物和80-100重量份的环氧树脂。基于总重量部分的100.0重量%,包含30-70重量%的溶剂。在混合步骤中,将粘结剂树脂组合物和无机化合物以1:1-3:1的重量比混合。; COPYRIGHT KIPO 2012

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