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METHOD FOR SYNTHESIS OF FULLERIDE METAL NANOCLASTER AND MATERIAL, INCLUDING FULLERIDE OF METAL NANOCLASTER

机译:合成金属纳米颗粒和材料的方法,包括金属纳米颗粒的方法

摘要

1. The method of synthesis of fulleride metal nanocluster, characterized in that! conduct mechanical fusion of metal nanoclusters with fullerene-type clusters, in which the fullerene molecules in the fulleride of the metal nanocluster are preserved. ! 2. The method according to claim 1, characterized in that the mechanical fusion is carried out by grinding in a planetary mill. ! 3. The method according to claim 1 or 2, characterized in that the use of nanopowder metal nanoclusters with a particle size between 5 and 60 nm. ! 4. The method according to claim 1 or 2, characterized in that the use of nanoclusters of aluminum-lithium alloy. ! 5. The method according to claim 1 or 2, characterized in that the planetary mill uses steel grinding balls having a weight between 250 and 270 g, and / or use steel grinding balls having a diameter between 6 and 8 mm. ! 6. The method according to claim 1 or 2, characterized in that the mechanical fusion is carried out in an atmosphere comprising argon and hydrogen. ! 7. The method according to claim 1 or 2, characterized in that metal nanoclusters and fullerene type clusters are used in granules with a size between 0.5 and 0.6 mm. ! 8. The method according to claim 1 or 2, characterized in that metal nanoclusters and fullerene-type clusters are used, comprising between 95 and 99% by weight of metal nanoclusters and between 5 and 1% by weight of fullerene. ! 9. The method according to claim 2, characterized in that grinding balls and acceleration of grinding balls between 800 and 1200 m / s2 are used. ! 10. The method according to claim 1 or 2, characterized in that the grinding of metal nanoclusters is carried out for a time between 80 and 120 minutes, and the grinding of metal nanoclusters with fullerene is performed for a time between 10 and 30 minutes or grinding
机译:1.合成富勒烯金属纳米簇的方法,其特征在于!进行富勒烯型簇的金属纳米簇的机械融合,其中保留了金属纳米簇的富勒烯中的富勒烯分子。 ! 2.根据权利要求1所述的方法,其特征在于,所述机械熔合通过在行星式磨机中进行研磨来进行。 ! 3.根据权利要求1或2所述的方法,其特征在于,使用粒度在5至60nm之间的纳米粉末金属纳米簇。 ! 4.根据权利要求1或2所述的方法,其特征在于,使用铝-锂合金的纳米团簇。 ! 5.根据权利要求1或2所述的方法,其特征在于,所述行星磨机使用重量在250至270g之间的钢磨球,和/或使用直径在6至8mm之间的钢磨球。 ! 6.根据权利要求1或2所述的方法,其特征在于,所述机械熔融是在包含氩气和氢气的气氛中进行的。 ! 7.根据权利要求1或2所述的方法,其特征在于,将金属纳米团簇和富勒烯型团簇用于粒度在0.5至0.6mm之间的颗粒中。 ! 8.根据权利要求1或2所述的方法,其特征在于,使用金属纳米团簇和富勒烯型团簇,其包含95至99重量%的金属纳米团簇和5至1重量%的富勒烯。 ! 9.根据权利要求2所述的方法,其特征在于,使用的研磨球和研磨球的加速度在800和1200m / s2之间。 ! 10.根据权利要求1或2所述的方法,其特征在于,金属纳米团簇的研磨进行80至120分钟的时间,并且用富勒烯进行金属纳米团簇的研磨10至30分钟的时间或打磨

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