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METHOD FOR SYNTHESIS OF FULLERIDE METAL NANOCLASTER AND MATERIAL, INCLUDING FULLERIDE OF METAL NANOCLASTER
METHOD FOR SYNTHESIS OF FULLERIDE METAL NANOCLASTER AND MATERIAL, INCLUDING FULLERIDE OF METAL NANOCLASTER
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机译:合成金属纳米颗粒和材料的方法,包括金属纳米颗粒的方法
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摘要
1. The method of synthesis of fulleride metal nanocluster, characterized in that! conduct mechanical fusion of metal nanoclusters with fullerene-type clusters, in which the fullerene molecules in the fulleride of the metal nanocluster are preserved. ! 2. The method according to claim 1, characterized in that the mechanical fusion is carried out by grinding in a planetary mill. ! 3. The method according to claim 1 or 2, characterized in that the use of nanopowder metal nanoclusters with a particle size between 5 and 60 nm. ! 4. The method according to claim 1 or 2, characterized in that the use of nanoclusters of aluminum-lithium alloy. ! 5. The method according to claim 1 or 2, characterized in that the planetary mill uses steel grinding balls having a weight between 250 and 270 g, and / or use steel grinding balls having a diameter between 6 and 8 mm. ! 6. The method according to claim 1 or 2, characterized in that the mechanical fusion is carried out in an atmosphere comprising argon and hydrogen. ! 7. The method according to claim 1 or 2, characterized in that metal nanoclusters and fullerene type clusters are used in granules with a size between 0.5 and 0.6 mm. ! 8. The method according to claim 1 or 2, characterized in that metal nanoclusters and fullerene-type clusters are used, comprising between 95 and 99% by weight of metal nanoclusters and between 5 and 1% by weight of fullerene. ! 9. The method according to claim 2, characterized in that grinding balls and acceleration of grinding balls between 800 and 1200 m / s2 are used. ! 10. The method according to claim 1 or 2, characterized in that the grinding of metal nanoclusters is carried out for a time between 80 and 120 minutes, and the grinding of metal nanoclusters with fullerene is performed for a time between 10 and 30 minutes or grinding
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