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METHOD FOR ELECTRON-MICROPROBE CHEMICAL U-Th-Pb-DATING OF MINERAL CONCENTRATORS OF URANIUM AND THORIUM RADIOACTIVE ELEMENTS

机译:铀和T放射性元素矿物集中体的电子探针化学U-Th-Pb定年方法

摘要

FIELD: chemistry.;SUBSTANCE: sample preparation is carried out by making polished specimens or attaching separate mineral grains extracted from rocks to a filler-holder with subsequent opening of the crystals, grinding and polishing their surfaces and sputtering with carbon; images of the samples are obtained and analysed in back scattered electrons (BSE) using a microprobe analyser at accelerating potential of 15 kV and electron beam current of 30 nA; energy-dispersion spectra are obtained and analysed at accelerating potential of 15 kV and electron beam current of 30 nA; distribution maps of U, Th, Pb, Y and basic elements of the mineral-geochronometer matrix are obtained and analysed at accelerating potential of 15 kV and electron beam current of 80-250 nA depending on the mineral; qualitative and quantitative analysis of the composition of the mineral-geochronometers is carried out at accelerating potential of 15 kV and electron beam current of 250 nA; analytical data are recorded and the age of the minerals is obtained.;EFFECT: high accuracy of the method for electron-microprobe chemical U-Th-Pb-dating of mineral-concentrators of uranium and thorium radioactive elements.;3 dwg
机译:领域:化学;物质:通过制备抛光的样品或将从岩石中提取的单独的矿物颗粒附着到填充物支架上,随后打开晶体,对其表面进行研磨和抛光并用碳溅射,来进行样品制备;获得样品的图像并使用微探针分析仪在反向散射电子(BSE)中以15 kV的加速电势和30 nA的电子束电流进行分析。在15 kV的加速电位和30 nA的电子束电流下获得并分析了能量色散谱。根据矿物的不同,在15 kV的加速电势和80-250 nA的电子束电流下,获得并分析了矿物-地钟仪矩阵的U,Th,Pb,Y和基本元素的分布图;在15 kV的加速电位和250 nA的电子束电流下,对矿物地球精密计时器的组成进行定性和定量分析。记录:分析数据并获得矿物的年龄。效果:该方法对铀和mineral放射性元素矿物集中器的电子-微探针化学U-Th-Pb定年方法具有很高的准确性; 3 dwg

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