首页> 外国专利> Coating catalyst shaped body, by providing substrate having first end surface, second end surface and flow channels, and introducing suspension and/or solution in flow channels starting from first end surface

Coating catalyst shaped body, by providing substrate having first end surface, second end surface and flow channels, and introducing suspension and/or solution in flow channels starting from first end surface

机译:通过提供具有第一端面,第二端面和流动通道的基材,并在从第一端面开始的流动通道中引入悬浮液和/或溶液,从而涂覆催化剂成型体

摘要

The method comprises: providing a substrate (10) having a first end surface (12), a second end surface (14) and flow channels (16), which pass through the substrate from the first end surface to the second end face; placing the substrate in such a way that the flow channels are aligned in an angle of inclination to vertical; and introducing a suspension and/or solution (40) in the flow channels starting from the first end surface. The flow channels are parallely arranged to each other, where the angle of inclination is 90[deg] and is adjusted in a range of 45-90[deg] or in a range of 70-90[deg] . The method comprises: providing a substrate (10) having a first end surface (12), a second end surface (14) and flow channels (16), which pass through the substrate from the first end surface to the second end face; placing the substrate in such a way that the flow channels are aligned in an angle of inclination to vertical; and introducing a suspension and/or solution (40) in the flow channels starting from the first end surface. The flow channels are parallely arranged to each other, where the angle of inclination is 90[deg] , and is adjusted in a range of 45-90[deg] or in a range of 70-90[deg] . The suspension and/or solution: contains a catalytic active component or a precursor of a catalytic active component; and is introduced in the flow channel over the second end face or up to a filling limit, which is reached between first and the second end face and/or passes transverse or perpendicular to the flow channels. The introducing step is performed by pumping the suspension and/or solution into the flow channels. A counteracting pressure is produced in the flow channels. The suspension and/or solution has a viscosity of greater than 1 Pa seconds. The flow channels are closed at the second end surface. The counteracting pressure is applied to the flow channels coming from or adjacent to the second end surface. A capillary system is arranged before the first end surface and/or adjacent to the first end surface. The method further comprises: deriving an excess suspension and/or solution from the flow channels; drying the coated substrate; calcining the coated substrate at 300-900[deg] C under air, vacuum, protective gas, inert gas or argon; and transferring the precursor of the catalytic active component into the catalytic active component. Element selected from the suspension, the substrate and the flow channels comprises a support material. The support material is an open-pore and/or inorganic support material. The substrate is the element selected from the shaped body with parallel flow channels, a honeycomb body, a cordierite honeycomb, a silicon carbide honeycomb, an aluminum titanate honeycomb and a metal honeycomb. An independent claim is included for a catalyst.
机译:该方法包括:提供具有第一端面(12),第二端面(14)和流道(16)的基板(10),第一端面(12),第二端面(14)和流动通道(16)从第一端面穿过基板到达第二端面。以这样的方式放置基板,以使流动通道相对于垂直方向倾斜一个角度;从第一端面开始在流动通道中引入悬浮液和/或溶液(40)。流动通道彼此平行布置,其中倾斜角度为90°,并在45-90°的范围内或在70-90°的范围内调节。该方法包括:提供具有第一端面(12),第二端面(14)和流道(16)的基板(10),第一端面(12),第二端面(14)和流动通道(16)从第一端面穿过基板到达第二端面。以这样的方式放置基板,以使流动通道相对于垂直方向倾斜一个角度;从第一端面开始在流动通道中引入悬浮液和/或溶液(40)。流动通道彼此平行地布置,其中倾斜角度为90°,并且在45-90°的范围内或在70-90°的范围内调节。所述悬浮液和/或溶液:包含催化活性组分或催化活性组分的前体;并在第二端面上方或直至填充极限处引入流动通道,该填充极限在第一端面与第二端面之间达到和/或横向或垂直于流动通道通过。引入步骤通过将悬浮液和/或溶液泵入流动通道中来进行。在流动通道中产生抵消压力。悬浮液和/或溶液的粘度大于1Pa·秒。流动通道在第二端面处封闭。反作用力施加到来自第二端面或邻近第二端面的流动通道。毛细管系统布置在第一端面之前和/或邻近第一端面。该方法进一步包括:从流动通道获得过量的悬浮液和/或溶液;干燥涂覆的基材;在空气,真空,保护气体,惰性气体或氩气下于300-900℃下煅烧涂覆的基材;将催化活性组分的前体转移到催化活性组分中。选自悬浮液,基材和流动通道的元件包括支撑材料。载体材料是开孔和/或无机载体材料。基材是选自具有平行流动通道的成形体,蜂窝体,堇青石蜂窝,碳化硅蜂窝,钛酸铝蜂窝和金属蜂窝的元素。包括对催化剂的独立权利要求。

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