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METHOD FOR PRODUCING ALKOXYLATED PHENOL RESIN-TYPE CROSSLINKING AGENT

机译:烷基化酚醛树脂型交联剂的生产方法

摘要

PROBLEM TO BE SOLVED: To provide a method for producing an alkoxylated phenol resin-type crosslinking agent for photoresist, not damaging the crosslinking agent property, having a high sensitivity, and being excellent in the alkali solubility property and the film property of a cured film.;SOLUTION: A method for producing an alkoxylated phenol resin-type crosslinking agent includes (I) heating alkylphenols and aldehydes in a solvent in the presence of a basic catalyst to produce a resol resin containing repeating units of formulae (A) and (B), and (II) further adding an alcohol and an acid catalyst and heating the mixture to convert ≥95 mol% of an alkanol group of the repeating unit (B) to an alkoxyalkyl group.;COPYRIGHT: (C)2013,JPO&INPIT
机译:解决的问题:提供一种用于光致抗蚀剂的烷氧基化酚醛树脂型交联剂的制备方法,该方法不损害交联剂的性质,具有高灵敏度,并且碱溶性和固化膜的膜性质优异。解决方案:制备烷氧基化酚醛树脂型交联剂的方法包括:(I)在碱性催化剂存在下在溶剂中加热烷基酚和醛,以制备含有式(A)和(B)重复单元的甲阶酚醛树脂。 (II)进一步加入醇和酸催化剂,并加热混合物以将≥95mol%的重复单元(B)的链烷醇基转化为烷氧基烷基。;版权所有:(C)2013,JPO&INPIT

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