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One type of red fluorescent powder for white LED and its preparation method
One type of red fluorescent powder for white LED and its preparation method
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机译:一种用于白光LED的红色荧光粉及其制备方法
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摘要
The present invention discloses a white-light LED red phosphor and method of manufacturing the same. The chemical formula of the phosphor is Ca 1-y-m-e-r Y y M m X x-p P p Z z N n : Eu e , R r , wherein 0.001‰¤y‰¤0.2,0.001‰¤m‰¤0.2,0.5‰¤x,z‰¤1.5, 0.001‰¤p‰¤0.1,2‰¤n‰¤4,0.01‰¤e‰¤0.2,0.001‰¤r‰¤0.1, M is selected from at least one of Sr, Ba, Sc, Li, Na and K; X is selected from at least one of B, Al and Ga, wherein Al is must; Z is selected from Si, V, and Nb, wherein Si is must; R is selected from at least one of Dy, Er, Tm, and Lu, wherein Dy is must. The manufacturing method comprises: Weighing the raw materials according to the chemical formula components in the structural formula (1) and stoichiometric ratio; sealing tightly after mixing them in a protective atmosphere, and then performing segmented roasting in the protective atmosphere adopting the normal-pressure high-temperature solid-state method, finally obtaining the white-light LED red phosphor after post-processing. The phosphor according to the present invention has features such as good chemical stability, high luminous efficiency, and good anti- luminous attenuation performance, etc. Further, this manufacturing method is easy to operate, pollution-free, and low cost.
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机译:本发明公开了一种白光LED红色荧光粉及其制造方法。磷光体的化学式为Ca 1-ymer Y y M m X xp P p Z z N n:Eu e,R r,其中0.001‰¤y‰¤0.2,0.001‰¤m‰¤0.2,0.5‰¤ x,z‰1.5,0.001‰p‰0.1,2‰n‰¤4,0.01‰e‰¤0.2,0.001‰r‰¤0.1,M选自Sr,Ba中的至少一种,Sc,Li,Na和K; X选自B,Al和Ga中的至少一种,其中Al是必须的; Z选自Si,V和Nb,其中Si是必须的; R选自Dy,Er,Tm和Lu中的至少一种,其中Dy是必须的。该制造方法包括:根据结构式(1)中的化学式成分和化学计量比称量原料;将其在保护气氛中混合后密封,然后在保护气氛中采用常压高温固态法进行分段焙烧,经过后处理,最终得到白光LED红色荧光粉。根据本发明的磷光体具有诸如化学稳定性好,发光效率高和抗发光衰减性能好等特征。此外,该制造方法易于操作,无污染且成本低。
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