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PROCESS FOR THE PREPARATION OF ILOPERIDONE USING A NOVEL INTERMEDIATE
PROCESS FOR THE PREPARATION OF ILOPERIDONE USING A NOVEL INTERMEDIATE
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机译:一种新型中间体制备氯哌立酮的方法
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摘要
The present invention provides a novel process for the preparation of iloperidone using a novel intermediate. Thus for example, reacting 4-(3-chloropropoxy)-3-methoxy benzaldehyde with methyl magnesium iodide in ether and the reaction mass was heated for 6 hours at reflux temperature, the mass was cooled to ambient temperature and poured into a mixture of ice, water and dilute hydrochloric acid to obtain l-[4-(3-chloropropoxy)-3-methoxyphenyl]ethanol.
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