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Process for growing single crystals of Copper (I) PENTAthiophosphate (V) iodide Cu6PS5I by technique of directional crystallization from the melt
Process for growing single crystals of Copper (I) PENTAthiophosphate (V) iodide Cu6PS5I by technique of directional crystallization from the melt
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机译:通过从熔体中定向结晶的技术来生长单铜五硫代磷酸五碘化铜(Cu6PS5I)的方法
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摘要
A process for growing single crystals of copper (I) pentathiophosphate (V) iodide CuPSI by technique of directional crystallization from the melt includes stage heating the evacuated quartz ampoules containing initial components copper, phosphorus, sulfur, and also pre-synthesized CuI in the desired stoichiometric ratio. Heating is carried out to a maximum temperature and the melt is maintained at this temperature for 24 h. with following growing single crystals. The maximum temperature of the synthesis is 1350 K. The growing is carried out with the growing rate of 3 mm/day in ampoules with the tapered end.
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机译:通过从熔体中定向结晶技术生长五硫磷酸铜(I)五碘化铜(V)碘化物CuPSI的单晶的方法包括阶段性加热排空的石英安瓿瓶,该安瓿瓶中包含初始组分铜,磷,硫以及预合成的所需的CuI化学计量比。加热至最高温度,并将熔体在此温度下保持24小时。随后生长的单晶。合成的最高温度为1350K。以锥形末端的安瓿以3 mm / day的生长速率进行生长。
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