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AUTOMATIC SOLID PHASE MICROEXTRACTION (SPME) SAMPLING APPARATUS

机译:自动固相微萃取(SPME)采样设备

摘要

Automatic solid phase microextraction (SPME) sampling apparatus with a mobile sampler arm (2) with a holder (15) for a probe (5) carrying the SPME fiber 9 and an intermediate bracket (6) for transferring the probe (5) between a probe storage tray (4) and the gas chromatograph injector (7). In the various probe handling stages, the probes are collected by magnetic means (20, 22, 33) attached to the end of the plunger (17) in the holder (15), at the free end of the holder's body (16) and at the lower end of the block (29b) for guiding the probe needle (8). Said magnetic means interact with a ferromagnetic connector (12) attached to one end of the SPME fiber (9) and with a ferromagnetic flange (13) attached to the end of the needle (8) containing the fiber in order to place the probe on the transfer bracket (6) or remove it therefrom. The apparatus can perform analyses on SPME fibers that have already been exposed, extract analytes from samples, and subsequently transfer them for desorption in the gas chromatograph in a fully automatic way.
机译:自动固相微萃取(SPME)采样设备,带有移动的采样器臂(2),该采样器具有用于携带SPME纤维9的探针(5)的支架(15)和用于在探针之间转移探针(5)的中间支架(6)。探针存储托盘(4)和气相色谱进样器(7)。在各个探针处理阶段中,探针通过磁性装置(20、22、33)收集,磁性装置固定在支架(15)中柱塞(17)的端部,支架主体(16)的自由端和块(29b)的下端有一个导针(8)。所述磁性装置与附接到SPME纤维(9)的一端的铁磁连接器(12)以及附接到附接于包含纤维的针(8)的端部的铁磁凸缘(13)相互作用,以便将探针放置在其上。或从中卸下传输支架(6)。该设备可以对已经暴露的SPME纤维进行分析,从样品中提取分析物,然后以全自动方式将它们转移到气相色谱仪中进行解吸。

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