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DOUBLE WALL CARBON NANOTUE AND METHOD FOR PREPARING SAME

机译:双壁碳纳米管及其制备方法

摘要

PURPOSE: A double-walled carbon nanotube using a supported catalyst and a manufacturing method thereof are provided to have high purity and high selectivity of double-walled carbon nanotubes among synthesized carbon nanotubes and to reduce deformity and increase crystallinity. CONSTITUTION: A manufacturing method of double-walled carbon nanotubes comprises the following steps: preparing a supported catalyst; synthesizing carbon nanotubes by concurrently injecting hydrocarbon gas and hydrogen gas while increasing the temperature of a reactor up to 900-1000 deg. Celsius after charging the supported catalyst; and synthesizing carbon nanotubes by injecting hydrogen gas after decreasing reactor temperature to 200 deg. Celsius. The supported catalyst is manufactured by plasticizing a catalyst solution in which metallic catalysts and support elements are mixed in the reactor at 500-800 deg. Celsius. The ratio of support element (Mg): metallic catalyst (Co): molybdenum system activator (Mo) is 0 99: x: 0.025. Here, 0.05=x=0.075.
机译:用途:提供一种使用担载催化剂的双壁碳纳米管及其制造方法,以在合成的碳纳米管中具有高纯度和高选择性的双壁碳纳米管,并减少变形和增加结晶度。组成:双壁碳纳米管的制造方法包括以下步骤:制备负载型催化剂;通过同时注入烃气和氢气,同时将反应器的温度提高到900-1000度,来合成碳纳米管。负载催化剂后摄氏;降低反应器温度至200℃后,注入氢气,合成碳纳米管。摄氏温度负载型催化剂通过增塑催化剂溶液来制造,其中金属催化剂和载体元素在反应器中以500-800度混合。摄氏温度载体元素(Mg):金属催化剂(Co):钼系活化剂(Mo)之比为0 99∶x∶0.025。在此,0.05≤x≤0.075。

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