首页> 外国专利> REDUCTION PROCESS OF NANOPARTICLES DOPED RARE EARTH ION AND NANOPARTICLES DOPED REDUCED RARE EARTH ION

REDUCTION PROCESS OF NANOPARTICLES DOPED RARE EARTH ION AND NANOPARTICLES DOPED REDUCED RARE EARTH ION

机译:纳米颗粒掺杂稀土离子的还原过程及纳米颗粒掺杂稀土离子的还原过程

摘要

PURPOSE: A reduction method of a rare earth ion doped nanoparticle is provided to easily reduce rare earth ions doped on the nanoparticle at a low temperature using an alkanoic acid based/amine-based mixed solvent, and to rapidly produce the nanoparticle which emits light with various colors by an instant reduction reaction. CONSTITUTION: A reduction method of a rare earth ion doped nanoparticle comprises the following steps: mixing a metal precursor with a solvent, and heat-processing the mixture at 150-300C for 5-130 minutes to obtain the rare earth ion doped nanoparticle; and stirring an alkanoic acid based/amine-based mixed solvent with the solution from the previous step. An alkanoic acid based solvent is selected from lauric acid, oleic acid, decanoic acid, or palmitic acid. An amine-based solvent is selected from propylamine, butyl amine, octhyl amine, decylamine, dodecylamine, hexadecylamine, or oleoylamine. The alkanoic acid based/amine-based mixed solvent contains the alkanoic acid based solvent and the amine-based solvent in a volume ratio of 1:150-5. [Reference numerals] (I) 1,2 dodecane tiol (DDT); (II) Hexadecylamine (HDA); (AA) Oleic acid (OA)
机译:目的:提供一种还原稀土离子的纳米粒子的还原方法,以使用链烷酸/胺基混合溶剂在低温下轻松还原掺杂在纳米粒子上的稀土离子,并快速制备出纳米粒子,并利用通过即时还原反应产生各种颜色。组成:一种稀土离子掺杂纳米粒子的还原方法,包括以下步骤:将金属前驱体与溶剂混合,然后在150-300℃下热处理该混合物5-130分钟,得到稀土离子掺杂纳米粒子。将链烷酸/胺基混合溶剂与前一步骤的溶液一起搅拌。链烷酸基溶剂选自月桂酸,油酸,癸酸或棕榈酸。胺基溶剂选自丙胺,丁胺,辛胺,癸胺,十二烷胺,十六烷胺或油酰胺。链烷酸基/胺基混合溶剂包含链烷酸基溶剂和胺基溶剂的体积比为1:150-5。 [附图标记](I)1,2十二烷三醇(DDT); (II)十六烷基胺(HDA); (AA)油酸(OA)

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