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REDUCTION PROCESS OF NANOPARTICLES DOPED RARE EARTH ION AND NANOPARTICLES DOPED REDUCED RARE EARTH ION
REDUCTION PROCESS OF NANOPARTICLES DOPED RARE EARTH ION AND NANOPARTICLES DOPED REDUCED RARE EARTH ION
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机译:纳米颗粒掺杂稀土离子的还原过程及纳米颗粒掺杂稀土离子的还原过程
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摘要
PURPOSE: A reduction method of a rare earth ion doped nanoparticle is provided to easily reduce rare earth ions doped on the nanoparticle at a low temperature using an alkanoic acid based/amine-based mixed solvent, and to rapidly produce the nanoparticle which emits light with various colors by an instant reduction reaction. CONSTITUTION: A reduction method of a rare earth ion doped nanoparticle comprises the following steps: mixing a metal precursor with a solvent, and heat-processing the mixture at 150-300C for 5-130 minutes to obtain the rare earth ion doped nanoparticle; and stirring an alkanoic acid based/amine-based mixed solvent with the solution from the previous step. An alkanoic acid based solvent is selected from lauric acid, oleic acid, decanoic acid, or palmitic acid. An amine-based solvent is selected from propylamine, butyl amine, octhyl amine, decylamine, dodecylamine, hexadecylamine, or oleoylamine. The alkanoic acid based/amine-based mixed solvent contains the alkanoic acid based solvent and the amine-based solvent in a volume ratio of 1:150-5. [Reference numerals] (I) 1,2 dodecane tiol (DDT); (II) Hexadecylamine (HDA); (AA) Oleic acid (OA)
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