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Manufacturing method of Te and bismuth telluride nano tubes by solvothermal synthesis
Manufacturing method of Te and bismuth telluride nano tubes by solvothermal synthesis
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机译:溶剂热合成碲化铋铋纳米管的制备方法
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摘要
PURPOSE: A tellurium nanotube of solvothermal synthesis and a manufacturing method of bismuth telluride are provided to manufacture Te nano-tube by reacting a high-boiling point organic solvent, coupling agent, and Tellurium compound and to mass produce Bi2Te3 nano-tubes. CONSTITUTION: A tellurium nanotube of solvothermal synthesis comprises the following steps: manufacturing a mixed solution by mixing organic solvent with a coupling agent; and reacting tellurium compound in the mixture. The organic solvent is one or more kinds which are selected from ethylene glycol, oleic acid, oleylamine, hexadecane, ethylenediamine, dimethylformamide, pyridine, and acetone. The coupling agent is selected from polyviny pyrrolidone, polyvinylalcohol, cetyl-trimethyl-ammonium-bromide, ethylenediaminotetraacetic acid disodium salt, and sodium dodecyl-benzene-sulfonate. A manufacturing method of the Bi2Te3 nanotubes comprises a step of reacting a solution including bismuth compound and reducing agent with a solution which includes Te nano-tubes.
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机译:目的:提供一种溶剂热合成碲纳米管和碲化铋的制备方法,通过高沸点有机溶剂,偶联剂和碲化合物的反应制备Te纳米管,并大批量生产Bi2Te3纳米管。组成:溶剂热合成碲纳米管包括以下步骤:通过将有机溶剂与偶联剂混合制备混合溶液;使碲化合物在混合物中反应。有机溶剂是选自乙二醇,油酸,油胺,十六烷,乙二胺,二甲基甲酰胺,吡啶和丙酮中的一种或多种。偶联剂选自聚乙烯吡咯烷酮,聚乙烯醇,十六烷基三甲基溴化铵,乙二氨基四乙酸二钠盐和十二烷基苯磺酸钠。 Bi 2 Te 3纳米管的制造方法包括使包括铋化合物和还原剂的溶液与包括Te纳米管的溶液反应的步骤。
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