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METHOD FOR MANUFACTURING PALLADIUM-PLATINUM CORE SHELL CATALYST FOR FUEL CELL

机译:燃料电池用钯-铂核壳催化剂的制备方法

摘要

PROBLEM TO BE SOLVED: To provide a method for manufacturing a palladium-platinum core shell catalyst having higher catalyst activity and more excellent durability than a conventional catalyst.SOLUTION: A method has a constitution including (a) a stage for preparing a mixed solution by dissolving a palladium precursor and a surfactant into an organic solvent, (b) a stage for preparing a sol mixed with palladium core nanoparticles by raising a temperature of a mixed solution under an inert gas atmosphere, (c) a stage for producing a mixture by mixing a platinum precursor solution with the sol, (d) a stage for producing nanoparticles having a palladium-platinum core shell shape by raising a temperature of the mixture under an inert gas atmosphere, (e) a stage for manufacturing a palladium-platinum core shell catalyst by allowing a carbon support medium to adsorb the nanoparticles having the palladium-platinum core shell shape, and (f) a stage for removing the surfactant from the palladium-platinum core shell catalyst.
机译:解决的问题:提供一种制备具有比常规催化剂更高的催化剂活性和更优异的耐久性的钯-铂核壳催化剂的方法。解决方案:该方法具有以下结构:(a)通过以下步骤制备混合溶液的步骤:将钯前体和表面活性剂溶解在有机溶剂中,(b)通过在惰性气体气氛下升高混合溶液的温度来制备与钯核纳米颗粒混合的溶胶的步骤,(c)通过以下步骤制备混合物的步骤:将铂前体溶液与溶胶混合,(d)通过在惰性气体气氛下升高混合物的温度来生产具有钯-铂核壳形状的纳米粒子的阶段,(e)用于制造钯-铂核的阶段通过使碳载体介质吸附具有钯-铂核壳形状的纳米颗粒,和(f)从钯中去除表面活性剂的阶段,制备壳催化剂-铂核壳催化剂。

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