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Nickel powder direct manufacturing method using hydrothermal synthesis method

机译:利用水热合成法的镍粉直接制造方法

摘要

PROBLEM TO BE SOLVED: To provide a method for directly producing nickel powder using a hydrothermal synthesis method, excellent in dispersibility and reduction rate.SOLUTION: Nickel powder is produced through the steps of: (a) preparing a mixture for hydrothermal synthesis, in which NiO, a pH regulator, PdCl, anthraquinone, PVP (polyvinyl pyrrolidone) and water are mixed; (b) charging the mixture for hydrothermal synthesis into a reaction container and then heating the mixture up to the water boiling point or more; (c) adding a reducing agent to the mixture heated in the (b) step to resolve the NiO and then reducing the NiO into Ni; (d) cooling a resultant product of a hydrothermal reaction in the (c) step; and (e) acquiring Ni powder by cleaning and drying the resultant product cooled in the (d) step.
机译:解决的问题:提供一种利用水热合成法直接生产镍粉的方法,该方法具有优异的分散性和还原率。解决方案:镍粉是通过以下步骤生产的:将NiO,pH调节剂,PdCl,蒽醌,PVP(聚乙烯吡咯烷酮)和水混合; (b)将用于水热合成的混合物装入反应容器中,然后加热至水沸点以上。 (c)向在(b)步骤中加热的混合物中加入还原剂以溶解NiO,然后将NiO还原成Ni; (d)在(c)步骤中冷却水热反应的所得产物; (e)通过清洗和干燥在(d)步骤中冷却的所得产物来获得Ni粉。

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