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Process for the production of 3,4 'dihydroxybenzophenone as an intermediate for the production of 3,4'diacetoxybenzophenone

机译:制备3,4'二羟基二苯甲酮作为中间体的制备方法,用于制备3,4'二乙酰氧基二苯甲酮

摘要

Meta - by reacting in the presence of protic acids and Lewis acids and phenolic hydroxy benzoic acid, and methods of synthesizing the 3,4 '-dihydroxy benzophenone. When the reaction was complete, to remove a proton acid and a Lewis acid, then contacted with ammonium hydroxide and water (temperature of 10 ℃ below) 3,4 '-dihydroxy-benzophenone of the reaction product and then filtered. Can then be reacted with an acetylating agent in the presence of activated carbon and inorganic acids, the filtration material to produce a 3,4 '-diacetoxy benzophenone.
机译:通过在质子酸和路易斯酸与酚羟基苯甲酸的存在下反应,生成3,4'-二羟基二苯甲酮的方法。当反应完成后,除去质子酸和路易斯酸,然后与氢氧化铵和水(温度低于10℃)接触反应产物的3,4'-二羟基二苯甲酮,然后过滤。然后可以在活性炭和无机酸的存在下,与乙酰化剂反应,过滤得到3,4'-二乙酰氧基二苯甲酮。

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