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Method for preparing aluminum—zirconium—titanium—carbon intermediate alloy

机译:铝-锆-钛-碳中间合金的制备方法

摘要

The present invention discloses a method for producing an aluminum-zirconium-titanium-carbon (Al—Zr—Ti—C) intermediate alloy; the Al—Zr—Ti—C intermediate alloy comprises 0.01% to 10% Zr, 0.01% to 10% Ti, 0.01% to 0.3% C, and Al in balance; the producing method comprising the steps of: preparing commercially pure aluminum, zirconium, titanium, and graphite material according to the weight percentages of the aluminum-zirconium-titanium-carbon intermediate alloy; the graphite powder is subjected to the following treatments: being added to the aqueous solution of KF, NaF, K2ZrF6, K2TiF6 or the combination thereof, soaked for 12 to 72 hours, filtrated or centrifuged, and dried at 80° C. to 200° C. for 12 to 24 hours; melting the commercially pure aluminum and keeping it at 700° C. to 900° C. to provide aluminum liquid, in which the prepared zirconium, the titanium and the treated graphite powder are added and melted to provide an alloy solution; and keeping the alloys solution at 700° C. to 900° C. under agitation and performing casting molding. The present method produces a high-quality Al—Zr—Ti—C intermediate alloy in low cost.
机译:本发明公开了一种铝-锆-钛-碳(Al-Zr-Ti-C)中间合金的生产方法。 Al-Zr-Ti-C中间合金包括0.01%至10%的Zr,0.01%至10%的Ti,0.01%至0.3%的C和余量的Al;该生产方法包括以下步骤:根据铝-锆-钛-碳中间合金的重量百分比,制备商业上纯净的铝,锆,钛和石墨材料。将石墨粉进行以下处理:添加到KF,NaF,K 2 ZrF6,K 2 TiF 6 的水溶液中或其组合,浸泡12至72小时,过滤或离心,并在80℃至200℃下干燥12至24小时;将市售的纯铝熔融并保持在700℃至900℃以提供铝液,在其中添加制备的锆,钛和处理过的石墨粉并熔融以提供合金溶液;在搅拌下将合金溶液保持在700℃至900℃并进行铸塑。本方法以低成本生产了高质量的Al-Zr-Ti-C中间合金。

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