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ULTRASOUND ASSISTED PROCESS FOR SYNTHESIS OF CHALCONE.

机译:超声波合成查尔酮的方法。

摘要

The present invention discloses a energy efficient process for the synthesis of chalcone derivatives by using ultrasound energy. Chalcone was successfully synthesized at room temperature by conventional (NUS) and sonochemical method (US). Detailed structural characterizations demonstrate that the US synthesized chalcones, which was synthesized in 10 min, are more stable and lower in particle size than the NUS synthesized chalcone. Sonochemical synthesis (US) method has saved substantial energy (more than 88%) for the synthesis of chalcone. Thus, the sonochemical synthesis technique is fast, simple, convenient, time saving, economical, and environmentally benign method of chalcone synthesis. This method promises a future iargescale synthesis for many organic intermediates. In view of the above, it can be seen that several advantages of the invention are achieved and other advantageous results are attained. As various changes could be made in the above methods and compositions without departing from the scope of invention, it is intended that all matter contained in the above description shall be interpreted as illustrative and not in limiting sense.
机译:本发明公开了一种利用超声能量合成查尔酮衍生物的节能方法。查耳酮是在室温下通过常规(NUS)和声化学方法(US)成功合成的。详细的结构表征表明,与NUS合成查耳酮相比,在10分钟内合成的美国合成查耳酮更稳定且粒径更小。声化学合成(美国)方法为查尔酮的合成节省了大量能源(超过88%)。因此,声化学合成技术是查耳酮合成的快速,简单,方便,省时,经济和环境友好的方法。该方法有望用于许多有机中间体的未来大规模合成。鉴于以上内容,可以看出实现了本发明的几个优点,并且获得了其他有利的结果。由于可以在不脱离本发明范围的情况下对上述方法和组合物进行各种改变,因此意图是将上述描述中包含的所有内容解释为说明性的,而不是限制性的。

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