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Method for determining of total sulfur in the technical sample of coal, lignite and/or biomass

机译:煤炭,褐煤和/或生物质技术样品中总硫的测定方法

摘要

determination of total sulphur in the way technical sample hard coal, lignite and / or biomass is the preparation of the sample (5) through the fragmentation of grains of the sample (5) to a size of at least 1 mm,and then subjected to the surface of the sample (5) action niskoenergetycznego radiation x from the source (2) and co registering and computation of an induced x-ray radiation characteristic sulphur using the detector (3) where the radiation fluorescenc yjnego whose exit is coupled with wielokanau0142owym analyser (4),and the percentage share of total sulphur determination in the test sample (5). during irradiation the samples (5) distance from its upper surface detector (3) is maintained in the range of 3 to 10 mm.
机译:以技术样品硬煤,褐煤和/或生物质的测定方法是通过将样品(5)的颗粒破碎至至少1 mm的大小来制备样品(5),然后进行到样品(5)的表面,从源(2)发出niskoenergetycznego辐射x,并使用检测器(3)共配准和计算诱导的x射线辐射特征硫,其中辐射的荧光yjnego的出口与wielokana耦合 u0142owym分析仪(4),以及总硫含量测定在测试样品中的百分比(5)。在辐照期间,样品(5)与其上表面检测器(3)的距离保持在3至10 mm的范围内。

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