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Method for preparing phosphate Method for preparing isopropylphenyl phosphates with reduced content of triphenyl phosphate (TPP)
Method for preparing phosphate Method for preparing isopropylphenyl phosphates with reduced content of triphenyl phosphate (TPP)
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机译:制备磷酸盐的方法制备磷酸三苯酯(TPP)含量降低的异丙基苯基磷酸盐的方法
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摘要
the subject of the invention is a method of alkylphenol phosphate reduced trifenylowego phosphate (tpp) of phosphorus oxychloride and) reaction with a mixture of izopropylofenoli (ipf) in the presence of a catalyst, using an ipf to pocl3, and ii) reaction the resulting mixture of phenol, characterised by that the ipf to pocl3 ranges from 1.3 to 1.5.how does not require oddestylowywania pocl3 and controlling composition contains in the final 60 - 75 mpa x s.
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机译:本发明的主题是一种使烷基酚磷酸酯还原三氯氧磷的磷酸三氟代膦酸酯(tpp)的方法,并且)在催化剂的存在下,与异丙基茴香醚(ipf)的混合物反应,使用ipf生成pocl3,和ii)反应所得产物酚的混合物,其特征在于ipf与pocl3的范围为1.3至1.5。如何不需要奇异的低矮wania pocl3,并且控制组合物最终含有60-75 mpa x s。
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