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METHOD FOR PRODUCING SULFONYL AMIDE COMPOUND CONTAINING FLUORINATED ALIPHATIC GROUP AND METHOD FOR PRODUCING ANIONIC HYDROPHILIC GROUP-CONTAINING SURFACTANT
METHOD FOR PRODUCING SULFONYL AMIDE COMPOUND CONTAINING FLUORINATED ALIPHATIC GROUP AND METHOD FOR PRODUCING ANIONIC HYDROPHILIC GROUP-CONTAINING SURFACTANT
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机译:含氟烷基的酰胺基化合物的制备方法及阴离子型含亲水基的表面活性剂的制备方法
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摘要
The objective of the present invention is to provide a method for producing, at a high yield, a sulfonyl amide compound containing a fluorinated aliphatic group, the method comprising: a first step of adding a ketone compound (a1) having 5 to 10 carbon atoms and a diamine compound (a2) to an organic solvent (a3) such that the ratio of carbonyl groups (a1-1) in the ketone compound (a1) and amino groups (a2-1) in the diamine compound (a2) is in a range of 0.3 to 0.95 in [(a1-1)/(a2-1)] molar ratio, and reacting the ketone compound (a1) and the diamine compound (a2) in the organic solvent (a3) to obtain a compound (A) that contains an amino group and a ketimine group; a second step of reacting the compound (A) with a sulfonyl chloride compound (B) containing a fluorinated aliphatic group to obtain a fluorinated aliphatic group-containing compound (C) that has a ketimine group; and a third step of hydrolyzing the ketimine group in the compound (C) to generate an amino group in the compound (C).
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