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IMIDAZOLE COMPOUND PRODUCTION METHOD, IMIDAZOLE COMPOUND, IMIDAZOLE-BASED COMPOUND, ORGANIC METAL COMPLEX, MATERIAL FOR ORGANIC ELECTROLUMINESCENT ELEMENT, ORGANIC ELECTROLUMINESCENT ELEMENT, DISPLAY DEVICE, AND LIGHTING DEVICE
IMIDAZOLE COMPOUND PRODUCTION METHOD, IMIDAZOLE COMPOUND, IMIDAZOLE-BASED COMPOUND, ORGANIC METAL COMPLEX, MATERIAL FOR ORGANIC ELECTROLUMINESCENT ELEMENT, ORGANIC ELECTROLUMINESCENT ELEMENT, DISPLAY DEVICE, AND LIGHTING DEVICE
A manufacturing method of an imidazole compound represented by a formula (1) below includes reacting 1-arylimidazole with a halogen-atom substituted compound. For performing this reaction, in a reaction system, a mole number Nf(2) [mol] of the halogen-atom substituted compound and a total volume Vsol [liter] of an ether solvent having at most 5 carbon atoms satisfy a relationship of Vsol/Nf(2)≤3.;In the formula (1): R1 and R4 represent a substituent and the like; Z1 represents a group of atoms necessary for forming a hydrocarbon cyclic group and the like; R2 and R3 represent a bond, a hydrogen atom or an aromatic hydrocarbon group; Z2 represents a group of atoms necessary for forming a five-membered hydrocarbon ring and the like together with C-C; and m represents an integer of 1 to 5.
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机译:由下式(1)表示的咪唑化合物的制造方法包括使1-芳基咪唑与卤素原子取代的化合物反应。为了进行该反应,在反应体系中,卤素原子取代的化合物的摩尔数N f(2) Sub> [mol]和总体积V sol Sub> [升具有最多5个碳原子的醚溶剂的[]满足V sol Sub> / N f(2) Sub>≤3的关系。;在式(1)中:R 1 Sub>和R 4 Sub>表示取代基等。 Z 1 Sub>表示形成烃环基等所需的原子团。 R 2 Sub>和R 3 Sub>表示键,氢原子或芳族烃基; Z 2 Sub>表示与C-C一起形成五元烃环等所需的原子团。 m表示1到5的整数。
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