PURIFING METHODE FOR IONIC LIQUID EMI-BF4

摘要

The present invention relates to a purifying method for high purity ionic liquid 1-ethyl-3-methylimidazolium tetrafluoroborate (EMI-BF4) comprising: a step of preparing synthesized EMI-BF4 (1-ethyl-3-methylimidazolium tetrafluoroborate); a step of removing precipitates existing in the synthesized EMI-BF4 by passing the synthesized EMI-BF4 through a glass filter; a step of performing primary vacuum distillation on the EMI-BF4 in which precipitates are removed; a step of mixing a distilled water mixture and the EMI-BF4 in a predetermined ratio and extracting ionic liquids with a liquid/liquid continuous extraction process by an extraction solvent; a step of drying the extracted ionic liquid by removing moisture; and a step of performing secondary vacuum distillation on the dried EMI-BF4.;COPYRIGHT KIPO 2014; [Reference numerals] (AA) Filtration; (BB) Vacuum distillation (100mmHg ↓ 24hr, 10mmHg ↓ 24hr); (CC) Mixing with a distilled water in a predetermined ratio; (DD) Extracting for 48 hours by an extraction solvent (dichloromethane); (EE) Drying (MgSO_4 anhydrous) vacuum distillation (100mmHg ↓ 24hr, 1mmHg ↓ 48hr); (FF) High purity ionic liquid (Purified 1-ethyl-3-methylimidazolium tetrafluoroborate)