首页> 外国专利> BATCH TYPE DISTILLATION APPARATUS FOR THE PURIFICATION OF LACTIDE, AND THE DISTILLATION METHOD FOR THE PURIFICATION OF LACTIDE USING THE SAME

BATCH TYPE DISTILLATION APPARATUS FOR THE PURIFICATION OF LACTIDE, AND THE DISTILLATION METHOD FOR THE PURIFICATION OF LACTIDE USING THE SAME

机译:间歇式精馏装置,用于丙交酯的精制,以及用于精制丙交酯的蒸馏方法

摘要

The present invention relates to a batch-type distillation purification device for lactide and a distillation purification method for lactide using same and, more particularly, provides a batch-type distillation purification device that is used to purify a lactide monomer from a lactide-containing mixture, including a raw material supply unit that supplies a lactide-containing mixture as a raw material; a distillation tower that is supplied with the lactide-containing mixture from the raw material supply unit and has a tower bottom portion storage tank where the mixture is stored in a lower portion; a reboiler that is connected to the tower bottom portion storage tank of the distillation tower and is supplied with a liquid mixture in the tower bottom portion storage tank; and a tower upper condenser that is connected to a tower upper portion of the distillation tower and allows external reflux and recovery by condensing a gas phase supplied from the tower upper portion to maintain a flow state, in which the reboiler is a liquid film type evaporator having a conduction surface area expanded in the form of a thin film.
机译:本发明涉及用于丙交酯的间歇式蒸馏纯化装置和使用该间歇式蒸馏纯化装置的丙交酯的蒸馏纯化方法,更具体地,提供一种用于从含丙交酯的混合物中纯化丙交酯单体的间歇式蒸馏纯化装置。包括原料供应单元,该原料供应单元供应含丙交酯的混合物作为原料;蒸馏塔,其从原料供给单元被供给含丙交酯的混合物,并具有塔底部的储罐,混合物被储存在下部。再沸器,其连接至蒸馏塔的塔底部存储罐并在塔底部存储罐中被供给液体混合物;再沸器为液膜式蒸发器,塔上部冷凝器连接至蒸馏塔的塔上部,并且通过冷凝从塔上部提供的气相以维持流动状态而允许外部回流和回收。具有以薄膜形式扩展的导电表面积。

著录项

  • 公开/公告号KR20140083474A

    专利类型

  • 公开/公告日2014-07-04

    原文格式PDF

  • 申请/专利权人 KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY;

    申请/专利号KR20120153267

  • 发明设计人 KIM YEONG CHEOL;

    申请日2012-12-26

  • 分类号B01D3/28;B01D3/32;B01D3;C07D319/10;

  • 国家 KR

  • 入库时间 2022-08-21 15:42:34

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