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Method for preparing zirconium phosphate particles coated by antibiotic, and zirconium phosphate particles prepared thereby

机译:涂覆有抗生素的磷酸锆颗粒的制备方法,以及由此制备的磷酸锆颗粒

摘要

The present invention method for producing a coated phosphate antibacterial minutes zirconium phosphate coating powder and thereby the antibacterial substance produced by relates to a zirconium powder, according to the present invention (A) in de-ionized water zirconium phosphate (Zr (HPO 4 ) 2 and nH 2 O ) was placed in a basket mill (basket mill) to the reactor after the dispersion to a particle size of 500nm or less through, 20 to 60 steps of dispersing from 0.2 to 1 hours with stirring at ; (B) and in de-ionized water is the precursor ion, zinc, magnesium, and added dropwise to an aqueous solution obtained by dissolving any of the metal salt is selected from the group consisting of calcium and copper, 12 to 48 hours to react to form a zirconium phosphate having an antibacterial activity steps; (C) wherein (B) the filtration of the zirconium phosphate phase, washed with deionized water and hot-air drying to 4-12 hours in the far infrared dryer 45 ~ 120 ; And (D), and then grinding 250 ~ 300 from 0.5 to 1 hour, 450 to 1-2 hours of the zirconium phosphate powder prepared by the thermal decomposition minutes antimicrobial coating including forming a coating layer on the zirconium phosphate antibacterial substance at 500 method is provided. ;
机译:本发明的用于制备涂覆的磷酸盐抗菌分钟磷酸锆涂料粉末的方法,由此涉及一种根据本发明(A)的在去离子水磷酸锆(Zr(HPO 4 2 和nH 2 O)在分散至粒径为500nm或更小后,放入到反应器的篮式粉碎机(basket mill)中通过在搅拌下在0.2至1小时内分散20至60个步骤; (B)和在去离子水中的前体离子是锌,镁,并滴加到通过溶解任何金属盐而获得的水溶液中,选自钙和铜,反应12至48小时形成具有抗菌活性的磷酸锆步骤; (C)其中(B)过滤磷酸锆相,用去离子水洗涤,并在远红外干燥机45〜120中热风干燥至4-12小时; (D),然后在0.5至1小时,250至300至450小时至1-2小时的时间内研磨250〜300小时的磷酸锆粉末,该粉末通过热分解分钟进行抗菌涂层,包括以500法在磷酸锆抗菌物质上形成涂层提供。 ;

著录项

  • 公开/公告号KR101405092B1

    专利类型

  • 公开/公告日2014-06-10

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20120104857

  • 发明设计人 유대성;천종우;김동현;

    申请日2012-09-21

  • 分类号C01B25/37;C01G5/00;B01J2/00;

  • 国家 KR

  • 入库时间 2022-08-21 15:40:45

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