首页> 外国专利> COPPER NANOPARTICLE, COPPER NANOPARTICLE PASTE USING THE SAME, COPPER NANOPARTICLE CORE-SHELL METAL, COPPER NANOPARTICLE PRODUCTION APPARATUS AND COPPER NANOPARTICLE PRODUCTION METHOD

COPPER NANOPARTICLE, COPPER NANOPARTICLE PASTE USING THE SAME, COPPER NANOPARTICLE CORE-SHELL METAL, COPPER NANOPARTICLE PRODUCTION APPARATUS AND COPPER NANOPARTICLE PRODUCTION METHOD

机译:铜纳米颗粒,使用相同的铜纳米颗粒糊料,铜纳米颗粒核心壳金属,铜纳米颗粒生产装置和铜纳米颗粒生产方法

摘要

PROBLEM TO BE SOLVED: To solve the problem that continuous production of a copper nanoparticle by passing a reaction solution containing a copper salt, a dispersant and a reductant through a reaction tube laid in a place irradiated with microwaves tends to cause a stop of continuous production of the copper nanoparticle or significant variation in particle size of the copper nanoparticle due to formation of copper mirror and/or adhesion of deposited copper, preventing low-cost production of a copper nanoparticle in a high yield.SOLUTION: A continuous production method of a copper nanoparticle comprises dissolving copper hydroxide and copper nitrate in the same solvent, mixing the resultant solution with a polycarboxylic acid and diethylene glycol monobutyl ether(C8H18O3) or with 2-ethylhexanol(C8H18O) and dodecane(C12H26) as a dispersant and then hydrazine as a reductant for copper salts and passing the resultant reaction solution through a microwave irradiation cavity to produce a copper nanoparticle while preventing formation of copper mirror and adhesion of precipitation.
机译:解决的问题:为了解决通过使包含铜盐,分散剂和还原剂的反应溶液通过放置在被微波照射的地方的反应管中而连续生产铜纳米颗粒的问题,从而导致连续生产的停止。由于铜镜的形成和/或沉积的铜的粘附导致铜纳米颗粒的粒径变化或铜纳米颗粒粒径的显着变化,从而阻止了高产量地低成本生产铜纳米颗粒。铜纳米颗粒包括将氢氧化铜和硝酸铜溶解在相同的溶剂中,将所得溶液与多元羧酸和二甘醇单丁醚(C8H18O3)或与2-乙基己醇(C8H18O)和十二烷(C12H26)作为分散剂混合,然后与肼混合。铜盐的还原剂,并使所得反应溶液通过微波辐照腔,以产生铜每纳米粒子,同时防止形成铜镜和沉淀的粘附。

著录项

  • 公开/公告号JP2015059243A

    专利类型

  • 公开/公告日2015-03-30

    原文格式PDF

  • 申请/专利权人 SHINKO KAGAKU KOGYOSHO:KK;

    申请/专利号JP20130193774

  • 发明设计人 WATANABE KENICHI;KODA HIDEKAZU;

    申请日2013-09-19

  • 分类号B22F1;B22F9/24;H01B13;B82Y30;B82Y40;H01B5;

  • 国家 JP

  • 入库时间 2022-08-21 15:33:38

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