首页> 外国专利> Method for Preparing Size-Controlled Gold Nanoparticles and Colorimetric Detection Method of Strong Acid Using the Same

Method for Preparing Size-Controlled Gold Nanoparticles and Colorimetric Detection Method of Strong Acid Using the Same

机译:尺寸控制金纳米粒子的制备方法及使用强酸比色法检测强酸的方法

摘要

A method for preparing hydrophobic gold nanoparticles includes adding 1,2-dichlorobenzene as a solvent to gold precursor and using oleylamine and oleic acid with volume ratio of 7.5:2.5 to 5:5 as surfactants. The size of the prepared gold nanoparticles can be controlled over a broad range and may be utilized in various fields such as bio-imaging, photonic crystallization, sensors, organic catalysts, surface enhanced raman spectrum, electronic devices, etc. Further, a method for colorimetric detection of a strong acid uses hydrophilic nanoparticles that are phase transited from the prepared hydrophobic gold nanoparticles. Up to 5 ppm of low content hydrochloric acid can be detected utilizing phase transited hydrophilic nanoparticles in the colorimetric detection method, and the gold nanoparticles that were used in the detection of strong acid can be reused without loss of activity through neutralization with bases.
机译:制备疏水性金纳米颗粒的方法包括将1,2-二氯苯作为溶剂添加至金前体中,并使用体积比为7.5:2.5至5:5的油胺和油酸作为表面活性剂。所制备的金纳米颗粒的尺寸可以在宽范围内控制,并且可以用于各种领域,例如生物成像,光子结晶,传感器,有机催化剂,表面增强拉曼光谱,电子器件等。强酸的比色检测使用亲水性纳米颗粒,该亲水性纳米颗粒从制备的疏水性金纳米颗粒发生相变。在比色检测方法中,可以使用相转移的亲水性纳米颗粒检测高达5 ppm的低含量盐酸,并且通过与碱的中和,可以重用用于强酸检测的金纳米颗粒而不会损失活性。

著录项

  • 公开/公告号US2014377876A1

    专利类型

  • 公开/公告日2014-12-25

    原文格式PDF

  • 申请/专利权人 KOREA BASIC SCIENCE INSTITUTE;

    申请/专利号US201314087159

  • 发明设计人 GAE HANG LEE;YEON SUK CHOI;DOO RI BAE;

    申请日2013-11-22

  • 分类号G01N21/80;B22F1/00;B22F9/24;

  • 国家 US

  • 入库时间 2022-08-21 15:22:13

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