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Process for Production of Low Ash Clean Coal from High Ash Coal with Total Solvent Recovery
Process for Production of Low Ash Clean Coal from High Ash Coal with Total Solvent Recovery
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机译:从高灰分煤中回收总溶剂的低灰分清洁煤生产方法
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摘要
A process to produce low ash clean coal from high ash coal with substantially complete solvent recovery, the process including: forming a slurry of coal fines in a N-Methyl-2-pyrrolidone (NMP) and Ethylenediamine (EDA) solution; maintaining said slurry in a reactor at a temperature range of 100° C. to 240° C. and a pressure range of 1 to 4 gauge (kg/cm2) for a period of about 15 minutes to 4 hours; separating the produced sample withdrawn from the reactor, one part being a filtrate and the other a reject; feeding the filtrate into an evaporator to recover 80-85% solvent; precipitating the concentrated filtrate material in an anti-solvent tank to separate coal from solvent; separating the coal by filtration, said separated coal having a reduced ash content; feeding the anti-solvent and solvent mixture into a distillation column to separate remaining solvent from the anti-solvent for reuse in the process.
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机译:一种由高灰分煤生产的具有低灰分纯度的煤并具有基本完全的溶剂回收能力的工艺,该工艺包括:在N-甲基-2-吡咯烷酮(NMP)和乙二胺(EDA)溶液中形成煤细粉的浆液;将所述浆料在反应器中在100℃至240℃的温度范围和1至4表压(kg / cm 2)的压力范围内保持约15分钟至4小时的时间;分离从反应器中取出的生产样品,其中一部分为滤液,另一部分为废品;将滤液送入蒸发器以回收80-85%的溶剂;在反溶剂罐中沉淀浓缩的滤液物质,以将煤与溶剂分离;通过过滤分离煤,所述分离的煤具有降低的灰分含量;将反溶剂和溶剂的混合物进料到蒸馏塔中,以从反溶剂中分离剩余的溶剂,以在工艺中重复使用。
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