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A PROCESS FOR DIRECT LIQUEFACTION OF COAL

机译:煤直接液化的方法

摘要

The present invention relates to a process for direct coal liquefaction of coal. The process comprises: (1) preparing a coal slurry from raw coal; (2) preheating the coal slurry, then feeding it into a reaction system to undergo liquefaction reaction; (3) separating reaction products in a separator (9, 10) to form a liquid phase and a gas phase, wherein the liquid phase is fractionated in an atmospheric tower (11) into a light oil fraction and a bottom product; (4) feeding the atmospheric tower bottom product to a vacuum tower (12) to separate into distillate and vacuum residue; (5) mixing the light oil fraction and the distillate to form a mixture, then feeding the mixture to a suspended bed hydrotreating reactor (13) with forced circulation for hydrogenation; (6) fractionating hydrogenation products into oil products and a hydrogen donor recycling solvent. The process could be operated steadily over a long period of time, with higher reactor efficiency and utilization factor. It could prevent mineral salts sedimentation and be operated under mild reaction conditions, therefore, the liquid oil yield could be increased and high-quality feedstock for further processing could be supplied.
机译:煤炭直接液化的方法技术领域本发明涉及煤炭直接液化的方法。该方法包括:(1)从原煤制备煤浆; (2)将煤浆预热后,送入反应体系进行液化反应。 (3)在分离器(9、10)中分离反应产物以形成液相和气相,其中在常压塔(11)中将液相分馏成轻油馏分和塔底产物; (4)将常压塔底产物送入真空塔(12)以分离成馏出物和真空残余物; (5)将轻油馏分和馏出液混合形成混合物,然后将混合物加到强制循环的悬浮床加氢处理反应器(13)中进行氢化; (6)将加氢产物分馏成油产物和供氢体再循环溶剂。该方法可以长时间稳定运行,具有更高的反应器效率和利用率。它可以防止矿物盐沉淀,并在温和的反应条件下运行,因此,可以提高液体油的收率,并可以提供用于进一步加工的优质原料。

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