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Method for obtaining polymer carrier of complex catalysts and method for obtaining complex catalyst heterogenized on this carrier

机译:获得络合物催化剂的聚合物载体的方法和获得在该载体上异质化的络合物催化剂的方法

摘要

process to obtain a polymer carrier complex catalysts, is that the resin tioepoksydowu0105 subjected u017celowaniu utwardzaczem politiouretanowym in presence of accelerator using the appropriate quantity utwardzacza and accelerator per 100 parts by weight of the resin, after which utwardzonu0105 resin is frozen in liquid nitrogen and breaks up into powder form.process to obtain a catalyst complex heterogenizowanego in this medium is that the medium is mixed with a solution of palladium or platinum in toluene, hexane, chloroform, methylene chloride or ethyl acetate, in terms nadkrytycznego carbon dioxide by answering ednim relation weight medium and metal complex solution, after which the resulting product oozes,washed several times to remove the unreacted toluene complex metal and dried under vacuum.
机译:聚合物载体配合物催化剂的方法是,在促进剂的存在下,使用适当量的utwardzacza和促进剂,每100重量份树脂对树脂tioepoksydow u0105进行 u017celowaniu utwardzaczem politiouretanowym,然后将utwardzon u0105树脂冷冻液态氮分解成粉末状。在该介质中获得催化剂配合物的方法是将介质与钯或铂在甲苯,己烷,氯仿,二氯甲烷或乙酸乙酯中的溶液混合,用nadkrytycznego二氧化碳表示通过回答埃迪尼姆关系重量介质和金属络合物溶液,然后将所得产物渗出,洗涤数次以除去未反应的甲苯络合物金属并真空干燥。

著录项

  • 公开/公告号PL405622A1

    专利类型

  • 公开/公告日2015-04-27

    原文格式PDF

  • 申请/专利权人 POLITECHNIKA ŁÓDZKA;

    申请/专利号PL20130405622

  • 发明设计人 NATALIA BĄCZEK;KRZYSZTOF STRZELEC;

    申请日2013-10-14

  • 分类号B01J32/00;B01J31/06;B01J23/42;B01J23/44;

  • 国家 PL

  • 入库时间 2022-08-21 15:13:17

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