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PROCESS FOR PREPARING A COMPLEX FERTILIZER WITH CONTROLLED RELEASE

机译:具有受控释放的复合肥料的制备方法

摘要

The invention relates to a process for preparing a complex fertilizer with controlled release. According to the invention, the process consists in pre-polymerizing a solution of pre-condensate of urea-formaldehyde and industrial urea granules at a formaldehyde : urea molar ratio of 0.75...1.5 : 1, while stirring and heating continuously for 2 h, at a temperature of 65...95°C, at a pH value of 8.5...9.5, by periodically dosing KOH or trisodic phosphate, after which the reaction mass is cooled down to the ambient temperature and an emulsion is admixed, the emulsion consisting of usual organic solvents and an aqueous solution containing 5...30% industrial glycerine and inorganic salts of N, P, K nutrients, the so formed emulsion being then admixed with urea up to a final urea : formaldehyde ratio of 1.65...2.4 : 1 and subjected to controlled heating at a temperature of 60...100°C, for 2 h, while correcting the pH to 2.5...4.5, after which the fertilizing precipitate is filtered at the ambient temperature and dried up to a constant mass.
机译:本发明涉及一种控制释放的复合肥料的制备方法。根据本发明,该方法包括以甲醛:尿素摩尔比为0.75 ... 1.5∶1的方式将脲-甲醛和工业尿素颗粒的预缩合物的溶液预聚合,同时搅拌并连续加热2小时。在65 ... 95°C的温度下,pH值为8.5 ... 9.5的条件下,定期添加KOH或三方磷酸盐,然后将反应物料冷却至环境温度,并混合乳液,由常规有机溶剂和含有5 ... 30%工业甘油和N,P,K营养素无机盐的水溶液组成的乳液,然后将如此形成的乳液与尿素混合,直至尿素与甲醛的最终比率为1.65 ... 2.4:1并在60 ... 100°C的温度下进行受控加热2小时,同时将pH值校正为2.5 ... 4.5,然后在环境温度下过滤施肥沉淀干燥至恒定质量。

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