首页> 外国专利> METHOD FOR PROVIDING A PURIFIED CRUDE GASEOUS C4 FRACTION AS AN INPUT STREAM FOR AN EXTRACTIVE DISTILLATION USING A SELECTIVE SOLVENT

METHOD FOR PROVIDING A PURIFIED CRUDE GASEOUS C4 FRACTION AS AN INPUT STREAM FOR AN EXTRACTIVE DISTILLATION USING A SELECTIVE SOLVENT

机译:提供一种纯化的粗气相G4馏分作为使用选择性溶剂进行萃取精馏的输入流的方法

摘要

The invention relates to a method for providing a purified crude gaseous C4 fraction (2) as an input stream for an extractive distillation using a selective solvent in order to obtain crude 1,3-butadiene on the basis of a liquid crude C4-fraction (1) as a feed stream, containing C3 hydrocarbons, C4 oligomers, C4 polymers, and C5+ hydrocarbons together with butanes, butenes, and 1,3-butadiene. The method has the steps of 1) separating the C4 oligomers, C4 polymers, and C5+ hydrocarbons up to the respective residual content previously specified for the purified crude gaseous C4 fraction and 2) evaporating the liquid crude C4 fraction in an evaporator tank (VK). The invention is characterized in that the evaporator tank (VK) is associated with a stripping column (K) with one or more separating stages, the liquid C4 fraction (1) being fed to the stripping column in the upper region of the stripping column. The stripping column directly exchanges gas and liquid with the evaporator tank (VK) in the lower region of the stripping column, and the purified crude gaseous C4 fraction (2) is drawn off from the stripping column in the upper region. The stripping column (K) is operated without a condenser at the column head.
机译:本发明涉及一种提供纯化的粗制气态C4馏分(2)作为输入物流的方法,该进料流使用选择性溶剂进行萃取蒸馏,以便基于液态的粗制C4馏分获得粗的1,3-丁二烯( 1)作为进料流,包含C3烃,C4低聚物,C4聚合物和C5 +烃以及丁烷,丁烯和1,3-丁二烯。该方法具有以下步骤:1)分离C4低聚物,C4聚合物和C5 +碳氢化合物,直至达到先前为纯化的粗制气态C4馏分指定的相应残余含量,和2)在蒸发罐(VK)中蒸发液态的粗制C4馏分。本发明的特征在于,蒸发罐(VK)与具有一个或多个分离级的汽提塔(K)相连,液体C4馏分(1)在汽提塔的上部区域中被供给到汽提塔。汽提塔与汽提塔下部区域中的蒸发罐(VK)直接交换气体和液体,纯化的粗制气态C4馏分(2)从汽提塔中上部区域排出。汽提塔(K)在塔头没有冷凝器的情况下运行。

著录项

  • 公开/公告号EP2802637A1

    专利类型

  • 公开/公告日2014-11-19

    原文格式PDF

  • 申请/专利权人 BASF SE;

    申请/专利号EP20130700159

  • 发明设计人 HEIDA BERND;HUGO RANDOLF;

    申请日2013-01-10

  • 分类号C10G21/28;C10G21/14;C10L3/12;B01D3/14;

  • 国家 EP

  • 入库时间 2022-08-21 15:05:00

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