首页> 外国专利> MICRO-MESOPOROUS CORE-SHELL COMPOSITE MOLECULAR SIEVE FOR REDUCING HARMFUL INGREDIENTS OF CIGARETTES AND PREPARATION METHOD THEREOF

MICRO-MESOPOROUS CORE-SHELL COMPOSITE MOLECULAR SIEVE FOR REDUCING HARMFUL INGREDIENTS OF CIGARETTES AND PREPARATION METHOD THEREOF

机译:减少香烟有害成分的微孔核壳复合分子筛及其制备方法

摘要

In the present invention, disclosed are a micro-mesoporous core-shell composite molecular sieve for reducing harmful ingredients of cigarettes and a preparation method thereof. The preparation method comprises the steps of: adding a template agent into a solution of which the alcohol-water ratio is 1:1 to 4:3; adding a zeolite molecular sieve; performing ultrasonic dispersion for 0.5-2 hours; dropping tetraethoxysilane of which the mass is 1-1.5 times that of the zeolite molecular sieve into the zeolite molecular sieve; stirring for 24-48 hours at room temperature; extracting a template agent using ethanol at normal temperature to obtain a mesoporous-microporous core-shell composite molecular sieve material. In the preparation method of the present invention, high-temperature calcination is omitted as the template agent is extracted directly using ethanol, and the preparation process is simpler. The micro-mesoporous core-shell composite molecular sieve is simple and convenient in operation and equipment requirements and low in price, and has good application prospect. Moreover, the micro-mesoporous core-shell composite molecular sieve has a significant adsorption effect on harmful substances especially phenol in smoke of cigarettes when being applied to a binary composite filter rod.;COPYRIGHT KIPO 2015
机译:在本发明中,公开了一种减少香烟有害成分的微孔核壳复合分子筛及其制备方法。该制备方法包括以下步骤:将模板剂添加至醇水比为1:1至4:3的溶液中;加入沸石分子筛;进行超声波分散0.5-2小时;将质量为沸石分子筛的1-1.5倍的四乙氧基硅烷滴加到沸石分子筛中;在室温下搅拌24-48小时;常温下用乙醇提取模板剂,得到中孔-微孔核-壳复合分子筛材料。在本发明的制备方法中,省去了高温煅烧,因为模板剂直接用乙醇提取,并且制备过程更简单。本发明的微孔核壳复合分子筛操作简便,设备要求低,价格低廉,具有良好的应用前景。此外,微介孔核-壳复合分子筛应用于二元复合滤嘴棒时,对香烟中有害物质特别是香烟中的苯酚具有显着的吸附作用。; COPYRIGHT KIPO 2015

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