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Treatment agent with excellentelasticity recovery and the the knitting textile treated therewith

机译:具有优异弹性回复率的处理剂和用其处理的针织物

摘要

The present invention relates to a fiber finishing agent having an improved elastic recovery rate and a fiber fabric knit treated with the finishing agent, wherein the fiber finishing agent having an improved elastic recovery rate comprises polytetramethylene ether glycols (PTMG) 3 to 4 and nitrosodiethanol Amine (NDEA, N-nitrosodiethanolamine) of 3.5 to 4, the internal temperature was increased to 70 to 80 ° C, and the mixture was allowed to react at a stirrer speed of 200 rpm for 30 minutes. Then, the reaction product of polytetramethylene glycol and nitrosodiethanolamine (IPDI, isophorone diisocyanate) was added at a molar ratio of 1: 0.9 to 1, dibutyl tin dilaurate (DBTDL) was added thereto, the temperature was lowered to 40 ° C, acetone was introduced, And the reaction was carried out for 3 hours while maintaining the temperature of the reaction system at 50 DEG C, and 35 to 40 mol% of hydrochloric acid (HCl) was added to 100 mol% After neutralization reaction for 3 hours, 18 to 25 mol% of ethylenediamine (EDA, Ethylen diamine) was added and chain extension reaction was carried out. When viscosity increased, acetone was added and stirred. When the neutralization reaction was completed, distilled water was slowly added for 3 hours, In water.
机译:本发明涉及一种具有提高的弹性回复率的纤维整理剂和一种用该整理剂处理的纤维织物,其中具有提高的弹性回复率的纤维整理剂包括聚四亚甲基醚二醇(PTMG)3至4和亚硝基二乙醇胺(NDEA,N-亚硝基二乙醇胺)为3.5至4,将内部温度升高至70至80℃,并使混合物在200rpm的搅拌器速度下反应30分钟。然后,以1:0.9:1的摩尔比加入聚丁二醇与亚硝基二乙醇胺的反应产物(IPDI,异佛尔酮二异氰酸酯),将二月桂酸二丁锡(DBTDL)加入其中,将温度降至40°C,将丙酮加热至室温。在保持反应体系温度为50℃的同时,进行反应3小时,并在100摩尔%中添加35〜40摩尔%的盐酸(HCl),中和反应3小时后,进行18小时。向其中加入25mol%的乙二胺(EDA,乙二胺)并进行扩链反应。当粘度增加时,加入丙酮并搅拌。中和反应完成后,将蒸馏水在水中缓慢加入3小时。

著录项

  • 公开/公告号KR101526931B1

    专利类型

  • 公开/公告日2015-06-11

    原文格式PDF

  • 申请/专利权人 한국생산기술연구원;

    申请/专利号KR20120114166

  • 发明设计人 조항성;이범수;허준;육지호;

    申请日2012-10-15

  • 分类号D06M15/37;D06M11/77;D06M13/332;

  • 国家 KR

  • 入库时间 2022-08-21 14:58:07

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