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METHOD FOR RAPID DETECTION OF EXPLOSIVES BASED ON ORGANIC PEROXIDES

机译:基于有机过氧化物的炸药快速检测方法

摘要

1. A method for rapid detection of explosives based on organic peroxides, based on the fixation liberated during the chemical decomposition of the hydrogen peroxide indicator method, characterized in that, before reacting the sample with an indicator is placed in contact with a solid phase material having surface acidity function and providing expansion an organic peroxide before the peroxide vodoroda.2. Method rapid detection of explosives based on organic peroxides according to claim 1, characterized in that the solid material has a surface acidity function protonating ability, preferably not less than that of concentrated sulfuric acid, and comprises at least a metal oxide superacid and / or high ftorsulfokisloty heterogeneous and / or acid in immobilized state on nanodispersed matritse.3 nanoporous polymer. Method rapid detection of explosives based on organic peroxides according to claim. 1, characterized in that as the indicator for the fixation of hydrogen peroxide used diammonium salt of 2,2'-azino-bis (3-etilbenztiazolil-6-sulfonic acid), 3.3 ', 5,5'-tetramethylbenzidine or a salt thereof, and to accelerate using horseradish peroxidase and / or peroxidase soi.4. Method rapid detection of explosives based on organic peroxides according to claim 1, characterized in that as an index used inorganic reducing agents, preferably selected from a number of iodine, potassium thiocyanate, titanila.5 sulfate. Method rapid detection of explosives based on organic peroxides according to claim 1,
机译:1.一种基于有机过氧化物的爆炸物的快速检测方法,其基于在过氧化氢指示剂方法的化学分解过程中释放的固定物,其特征在于,在使样品与指示剂反应之前,将其与固相材料接触。具有表面酸性功能,并在过氧化物香气膨胀之前提供有机过氧化物的膨胀; 2。 2.根据权利要求1所述的基于有机过氧化物的炸药快速检测方法,其特征在于,所述固体材料具有表面酸度功能的质子化能力,优选不小于浓硫酸的质子化能力,并且至少包含金属氧化物超酸和/或高氟磺基异位和/或酸固定在纳米分散的matritse.3纳米多孔聚合物上。 7.根据权利要求1的基于有机过氧化物的炸药的快速检测方法。 1,特征在于,作为过氧化氢的固定指示剂,使用2,2′-叠氮基双(3-etilbenztiazolil-6-磺酸),3.3′,5,5′-四甲基联苯胺的二铵盐或其盐。 ,并加快使用辣根过氧化物酶和/或过氧化物酶soi.4。 2.根据权利要求1所述的基于有机过氧化物的炸药的快速检测方法,其特征在于,使用无机还原剂作为指标,所述无机还原剂优选选自碘,硫氰酸钾,钛酸钛5硫酸盐。 2.根据权利要求1所述的基于有机过氧化物的炸药的快速检测方法

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