METHOD OF COMBINED OBTAINING OF 1,2-EPOXYDODECANE AND 1,2-DODECANEDIOL

摘要

FIELD: chemistry.;SUBSTANCE: target product represents 1,2-epoxydodecane and combined with it 1,2-dodecanediol, in a weight ratio of 3:1. The catalytic oxidation of 1-dodecen with sodium hypochlorite is carried out with the application of the catalyst KBr for 10 h in the presence of a solvent - acetonitrile, with a volume ratio 1-dodecene:acetonitrile, equal to 1:8÷15.;EFFECT: increased rate of carrying out the reaction and an increase of the target product output.;3 dwg, 2 tbl, 5 ex