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A method and equipment of producing graphite and metallic catalyst composite for diamond synthesis

机译:用于金刚石合成的石墨和金属催化剂复合物的生产方法和设备

摘要

This invention releases the preparation method and equipment of graphite and catalyst composite for a kind of synthetic diamond. Firstly the clean graphite particle shall be placed into the heating chamber (6) for pre-heating, the lower limit of the heating temperature shall be higher than the boiling point of the coated carbonyl metal complex und the upper limit of the heating temperature shall be set according to the thickness of the coating needed; secondly, the heated graphite particle will be fed into the coating room (7) with vibrator or agitator (11) and the steam of carbonyl metal complex shall be input for coating; finally the coated graphite particle shall be fed into the cooling and passivation room (8) for cooling and passivation of the discharging materials or enter the next round circle of heating and coating. As to the graphite and catalyst composite prepared by this invention, the surface of each graphite particle is plated with metal layer and the continuous metallic contact is formed between the particles of the synthetic cylinder prepared by it. In synthesis, it is easy to form the continuous metallic film so as to continuously feed the carbon to the diamond crystal nucleus to promote the crystal nucleus growing into perfect diamond crystal.
机译:本发明公开了一种合成金刚石的石墨和催化剂复合材料的制备方法和设备。首先将清洁的石墨颗粒放入加热室(6)中进行预热,加热温度的下限应高于被覆羰基金属配合物的沸点,加热温度的上限应为根据所需涂层的厚度进行设置;其次,将加热的石墨颗粒用振动器或搅拌器(11)送入涂覆室(7),并输入羰基金属配合物的蒸汽进行涂覆。最后,将涂覆的石墨颗粒送入冷却和钝化室(8),以对排放材料进行冷却和钝化,或者进入下一轮加热和涂覆。对于通过本发明制备的石墨和催化剂复合物,每个石墨颗粒的表面镀有金属层,并且在由此制备的合成圆筒的颗粒之间形成连续的金属接触。在合成中,容易形成连续的金属膜,以便将碳连续地供给到金刚石晶体核中,以促进晶体核生长成完美的金刚石晶体。

著录项

  • 公开/公告号EP1990089B1

    专利类型

  • 公开/公告日2016-03-30

    原文格式PDF

  • 申请/专利权人 JIANGSU TIANYI MICRO METAL POWDER CO LTD;

    申请/专利号EP20070123621

  • 发明设计人 KE ZUNBIN;WANG BIN;GAO WEIXIN;

    申请日2007-12-19

  • 分类号B01J13/06;B01J21/18;B01J23/34;B01J23/745;B01J23/75;B01J23/755;

  • 国家 EP

  • 入库时间 2022-08-21 14:52:04

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